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situ size control of the graphene size distribution during sonication. With further yield optimisation, the need for centrifugation could also be negated. Fig. 3 | Evidence that inertial cavitation preferentially exfoliated larger flakes during sonication. The mean graphene (a) length and (b) thickness as function of the ICD. The mean graphene (c) length and (d) thickness as a function of the graphene yield. The symbols in (a-d) delineate the data as function of sonication time, measured in minutes. The graphene exfoliation rate (𝑐𝑔/𝑡) as function of (e) the mean graphene length and (f) thickness for graphene samples produced with the highest and lowest pre-amp voltages (acoustic powers) used in this work. The uncertainty in the graphene yield and exfoliation rate is associated with the standard deviation of three graphene yield measurements at each sonication time, and the uncertainty in graphene length and thickness is associated with the standard error of ~300 and ~100 measurements, respectively. 10PDF Image | Cavitation Liquid Phase Exfoliation of Graphene
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