Graphene from Electrochemically Exfoliated Graphite

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Graphene from Electrochemically Exfoliated Graphite ( graphene-from-electrochemically-exfoliated-graphite )

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a) O-C=0 C=O C-O -C-C- -C=C- b) ROG OG EG 3700 3200 2700 2200 1700 1200 700 Wavenumber, cm-1 c) d) D G 0 20 40 60 .u.a ., Area, % u.a ecn ROG ,yti ati snet msn nI arT OG EG 281 283 285 287 289 291 293 295 Binding energy, eV .u. .u.a a, , yti ytis 0 10 20 30 40 sn ne 2 Theta (o) etnI tnI ROG OG EG Graphite D ́ (ID/IG)=1.61 (ID/IG)=1.76 (ID/IG)=1.41 (ID/IG)=0.1 OG ROG EG Graphite 0 10 20 2 Theta, (o) 30 40 1000 1200 1400 1600 1800 2000 Raman shift, cm-1 ROG OG EG Figure 3. (a) High-resolution core level C1s spectra (Inset shows the percentage (area) of different functional groups identified by deconvolution), (b) ATR-IR spectra of the samples obtained from the EEG process, (c) XRD patterns and (d) normalized Raman spectra. 25

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