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and 118. Copyright 2011 American Chemical Society, Copyright 2014 American Chemical Society. .......................................................................................................................................................... 105 Figure 24: a) Schematic representation of the electrochemical micro-reactor combining electrochemical exfoliation and shear-driven exfoliation. The graphite crystal is both the wall and the working electrode of the reactor and simultaneously experiences a high wall shear rate and an applied electric potential. Here H, Q, and are the height between two electrodes, electrolyte flow, and shear rate, respectively 54; b) Effect of potential and shear rate on the size of graphene flakes produced in the flow reactor. A mean size distribution of zero, specifically in the case for only potential and shear rate of 6925 s−1, indicates that exfoliation was unnoticed over the samples that were measured. The green and blue colors in the figure indicate shear and potential dominated regions, respectively. Statistical flake size analysis for the graphene was performed using more than 80 sheets from AFM measurements. Error bars in these figures are from three samples at a given condition, showing the maximum and minimum values. Reproduced with permission from ref. 54. Copyright 2016 American Chemical Society. ............................................................................................................................106 Figure 25: A summary of the top-down production considerations in the scale-up of graphene ....107 8PDF Image | graphene production via nonoxidizing liquid exfoliation
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