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3.3.2.1. Resistance-based strain sensors.............................................................96 3.3.2.2. Optical strain sensors..............................................................................98 3.3.2.2.1. Fibre optic sensors ............................................................................98 3.3.2.2.2. Photoelasticity-based sensors...........................................................99 4. METHODS...................................................................................................................102 4.1. Synthesis of graphene........................................................................................102 4.1.1. Micromechanical cleavage...........................................................................102 4.1.2. Liquid-phase exfoliated graphene ...............................................................102 4.1.2.1. 4.1.2.2. 4.1.2.3. General principles of ultrasonication ...................................................102 Experimental procedure .......................................................................103 Exfoliation in organic solvents ..............................................................105 4.1.2.3.1. Graphene paper preparation ..........................................................106 4.1.2.3.2. Size selection process......................................................................106 4.1.2.4. 4.1.2.5. 4.1.2.6. 4.1.2.7. Exfoliation in aqueous media using surfactants ...................................107 Exfoliation using lipids ..........................................................................108 Exfoliation using proteins .....................................................................109 Summary of different preparation methods ........................................110 4.1.3. Electrochemically exfoliated graphene........................................................110 4.1.4. CVD graphene ..............................................................................................111 4.1.5. Commercially sourced graphene .................................................................112 4.1.5.1. Elicarb® graphene .................................................................................112 4.1.5.2. Graphene supermarket CVD graphene ................................................112 4.1.6. Solvent exchange of graphene by dialysis ...................................................112 4.1.6.1. Dialysis principle ...................................................................................112 4.1.6.2. Dialysis experimental procedure ..........................................................113 5PDF Image | PRODUCTION AND APPLICATIONS OF GRAPHENE AND ITS COMPOSITES
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