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4.2. Preparation of typical graphene composite coatings ........................................114 4.2.1. Solution processed graphene/epoxy composites ........................................114 4.2.2. Mechanically-cleaved graphene composite coatings ..................................116 4.2.3. CVD graphene composite coatings ..............................................................117 4.3. Characterisation .................................................................................................118 4.3.1. Optical microscopy.......................................................................................118 4.3.2. Scanning electron microscope .....................................................................118 4.3.3. Atomic force microscope .............................................................................119 4.3.4. Dynamic Light Scattering .............................................................................119 4.3.4.1. 4.3.4.2. 4.3.4.3. DLS Principle .........................................................................................119 DLS experimental setup and procedure ...............................................122 Zeta potential........................................................................................123 4.3.5. Ultraviolet-visible spectroscopy...................................................................124 4.3.6. Fluorescence spectroscopy ..........................................................................125 4.3.7. Nuclear magnetic resonance spectroscopy .................................................125 4.3.8. X-ray diffraction ...........................................................................................126 4.3.9. Raman spectroscopy ....................................................................................126 4.3.9.1. Raman experimental setup...................................................................126 4.3.9.2. Deformational procedure .....................................................................128 5. PRODUCTION OF FEW LAYER GRAPHENE IN ORGANIC SOLVENTS .........................132 5.1. Introduction .......................................................................................................132 5.2. Production of FLG in organic solvents ...............................................................132 5.2.1. Effect of sonication time and centrifugation speed on the concentration of graphene ....................................................................................................................132 5.2.2. AFM characterisation...................................................................................135 6PDF Image | PRODUCTION AND APPLICATIONS OF GRAPHENE AND ITS COMPOSITES
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