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Acknowledgements This work was undertaken in the Chemical and Process Engineering Department (CAPE) of the University of Canterbury between March 2017 and August 2020. Funding for this work was gratefully received from the University of Canterbury Doctoral Scholarship and the MacDiarmid Institute. I am extremely thankful for the support and guidance of my supervisory team. My primary supervisor Associate Professor Dr Aaron Marshall. At every step he was approachable and innovative, enabling me to make progress and learn throughout my PhD experience. My co- supervisor, Professor Alison Downard, has a great understanding of electrochemistry and as a result led me to improve the clarity and quality of my work on numerous occasions. Without their support this thesis would not be what it is and I would certainly know a lot less about electrochemistry. The entire CAPE departmental staff have been a pleasure to work with, providing clear expectations and rigorous safety measures, with keen oversight from Rayleen Fredericks, Garrick Thorn and Michael Sandridge. Whenever I needed a new part or piece of equipment, the workshop technicians, Stephen Beuzenberg, Graham Furniss, Graham Mitchell and Leigh Richardson were efficient and easy to work with. I would like to give special thanks to Glenn Wilson for organising the repair of my potentiostat during a global pandemic. Ranee Hearst, Joanne Pollard and Rachel Rogers all helped me to solve various self-inflicted administration issues. Without the help of Ben Reynolds and Daniel Clarke it would not have been possible for me to write the code in Matlab to carry out the numerical simulations. I would also like to thank Wasim Khan for carrying out the BET measurements. Outside of CAPE, Anna Farquhar Paula Brooksby from the chemistry department were a great help for carrying out my early experiments. During my research I was lucky enough to use Raman spectra equipment at Massey University in Palmerston North, with help from Mark Waterland. Raman measurements were also taken at the University of Auckland with help from Rakesh Arul and the University of Otago by Chima Robert and Keith Gordon. iPDF Image | Electron Transfer Kinetics in Redox Flow Batteries
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