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5 Single fibre electrode measurements - a versatile strategy for assessing the non-uniform kinetics Using kinetic parameters measured at single carbon fibre electrodes and the void size distribution measured by CT imaging, the cyclic voltammetry of carbon felt electrodes was simulated using the numerical model described above (Section 3) and compared to experimental measurements over a range of sweep rates (Figure 5.4). It is important to note that simulated cyclic voltammograms describe the experimental data very well without requiring the use of any unconstrained fitting parameters (all inputs for the model were determined from CT and SEM imaging and the single fibre electrode measurements). Figure 5.4: Simulated cyclic voltammetry compared to experimental results in a solution of 0.1 mM ferricyanide and 0.1 mM ferrocyanide, at sweep rates of, a) 20 mV s-1 b) 50 mV s-1 c) 200 mV s-1. The simulated cyclic voltammograms use the calculated void distribution (Figure 3b) and the measured rate constant distribution (Table 5.1). 63PDF Image | Electron Transfer Kinetics in Redox Flow Batteries
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