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8 Half – cell performance of Carbon Felt Samples Polarization curve measurements were recorded at 15 mL min-1 for untreated and thermally treated GFE, G100 and C100 felts, (Figure 8.3). Figure 8.3: Polarization curves for each felt and thermal treatment, recorded in 0.4 M V4+ and 0.4 M V5+ dissolved in 3 M H2SO4. a) GFE felt samples, b) G100 felt samples and c) C100 felt samples. As expected the thermally treated GFE and G100 felts showed a clear reduction in overpotential, consistent with the trend in rate constants calculated in Chapter 7. Little change was observed for the thermally treated C100 felts, further supporting the accuracy of the apparent rate constants calculated from cyclic voltammetry in Chapter 7. 118PDF Image | Electron Transfer Kinetics in Redox Flow Batteries
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