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Extending organic flow batteries via redox state management

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Extending organic flow batteries via redox state management ( extending-organic-flow-batteries-via-redox-state-management )

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pH dependence of DHA 1H NMR spectrum In a nitrogen-filled glovebox, an aqueous solution of 0.1 M synthetic DHA and 1.2 M KOH was prepared. An 80 μL aliquot was then dissolved in 720 μL of D2O within a sealed , and the 1H NMR spectrum was obtained within 1 hour (top spectrum). A separate 80 μL aliquot was then dissolved in 720 μL of 1 M KOD in D2O, and the 1H NMR spectrum was obtained under identical conditions (bottom spectrum). Figure S11. 1H NMR spectra of DHA at pH 13 (top spectrum) and pH 14 (bottom spectrum). 5 mm Precision Low Pressure/Vacuum Valve (LPV) NMR tube (Wilmad-LabGlass Product No. 535-LPV-7) 13

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