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Chapter 4. Molecular Electrochemistry of Quinones Figure 4.18: (a) Cyclic voltammograms of 4 mM DHPA in 1 M KOH recorded on a GC WE at various scan rates, initially in the anodic direction. (b) Linear sweep voltammo- grams of 5mM DHPA in 1M KOH recorded on a GC WE at 5mVs−1 in the anodic direction and at rotation rates from 300–2500 rpm. The dashed grey line in each subplot represents a background recorded in blank solution, whereas the dashed vertical coloured lines represent the half-wave potentials of the sets of peaks observed in (a). Figure 4.19: Bulk electrolysis of 45 mL 5 mM DHPA in 1 M KOH recorded on a carbon mesh WE. The solution was first charged and discharged galvanostatically at ±25mA between potential limits of 0.44 and −0.21V vs. SHE (black lines) and then between potential limits of −0.54 and 0.34 V vs. SHE (red lines). Each half-cycle was followed by a potentiostatic hold at the limit until the current plateaued. 62PDF Image | Organic Redox Flow Batteries 2023
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