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List of Figures 130 6.9 Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1 M K4[Fe(CN)6] dissolved in 1 M KCl adjusted to pH 12, withoutandwithapulsationdampening.................... 97 6.10 Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1 M K4[Fe(CN)6] dissolved in 1 M KCl adjusted to pH 12, withoutandwithacontrolledtemperature.. . . . . . . . . . . . . . . . . 6.11 Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1M K4[Fe(CN)6] dissolved in 1M KCl adjusted to pH 12 before, during, and after controlling the temperature to 30 ◦C. . . . . . . 6.12 Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1M K4[Fe(CN)6] dissolved in 1M KCl adjusted to pH 12 andwithtemperaturesrangingfrom31◦Cto35◦C. . . . . . . . . . . . . 6.13 ResultsfromtheCNLSfitofthe0.1M/0.1Mferri-/ferrocyanideimpedance recorded at 31 ◦C. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6.14 Total, series, and resolved porous electrode resistances against cell tempe- rature for a 0.1M/0.1M ferri-/ferrocyanide system. . . . . . . . . . . . . . 98 . 99 . 100 . 100 . 101 6.15 Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1M K4[Fe(CN)6] dissolved in 1M KCl adjusted to pH 12 overatimeperiodof100h. ..........................102 6.16 Nyquist plots recorded on a one-container symmetric cell containing 0.1 M K3[Fe(CN)6]+0.1M K4[Fe(CN)6] dissolved in 1M KCl adjusted to pH 12 atflowratesrangingfrom10to90mLmin−1. . . . . . . . . . . . . . . . . 104 6.17 ResultsfromtheCNLSfitofthe0.1M/0.1Mferri-/ferrocyanideimpedance recorded at 50mLmin−1. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 104 6.18 Total, series, and resolved porous electrode resistances against flow rate for a 0.1M/0.1M ferri-/ferrocyanide system. . . . . . . . . . . . . . . . . . . . 105 6.19 Nyquist plots recorded on a one-container symmetric cell assembled with pretreated 1186HCBA electrodes and containing 0.1 M K3[Fe(CN)6]+0.1 M K4[Fe(CN)6] dissolved in 1M KCl adjusted to pH 12 with at flow rates rangingfrom10–90mLmin−1. .........................106 6.20 Nyquist plots recorded on a one-container symmetric cell containing 0.05 M DHAQ+0.05M DHAHQ dissolved in 1.2M KOH (= 1.0M OH–) in three successivemeasurementsandtheiraverage.. . . . . . . . . . . . . . . . . . 107 6.21 Nyquist plots recorded on a one-container symmetric cell containing 0.05 M DHAQ+0.05M DHAHQ dissolved in 1.2M KOH (= 1.0M OH–) at flow rates ranging from 10–90mLmin−1. . . . . . . . . . . . . . . . . . . . . . . 108 6.22 Results from the CNLS fit of the the 0.05 M DHAQ+0.05 M DHAHQ im- pedance recorded at 50mLmin−1. . . . . . . . . . . . . . . . . . . . . . . . 109 6.23 Total, series, and resolved porous electrode resistances against flow rate for a0.05MDHAQ+0.05MDHAHQsystem. ..................110 6.24 Nyquist plots recorded on a one-container symmetric cell containing 0.05 M DBEAQ+0.05 M DBEAHQ dissolved in 1.2 M KOH (= 1.0 M OH – ) at flow rates ranging from 10–90mLmin−1. . . . . . . . . . . . . . . . . . . . . . . 111 6.25 Results from the CNLS fit of the 0.05 M DBEAQ+0.05 M DBEAHQ impe- dancerecordedat50mLmin−1. ........................111 6.26 Total, series, and resolved porous electrode resistances against flow rate for a 0.05M DBEAQ+0.05M DBEAHQ system. . . . . . . . . . . . . . . . . . 112PDF Image | Organic Redox Flow Batteries 2023
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