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Appendix D SEM Images SEM images of Sigracet 39AA in pristine and pretreated (baked at 400 ◦C for 24 h) forms were taken to estimate the fibre diameter and pore size. This was done on a Carl Zeiss Merlin field emission scanning electron microscope, using an acceleration voltage of 5 kV, a probe current of 120 pA, and a gun-to-sample distance of 6.5 mm. Images were captured at magnifications of 800, 3,000, and 30,000 on a secondary detector, and are presented in Figure D.1. A fibre diameter of 7 μm was estimated, together with pore sizes in the range 50–120 μm for the pretreated sample. 147PDF Image | Organic Redox Flow Batteries 2023
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