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Figure 3.1. - Scheme of electrode synthesis processes over carbon felt (CF) i) oxygen plasma treatment. ii) Hydrothermal synthesis placing CF 1mg/mL in the reactor in H2O as solvent at 80oC for12h. iii) Hydrothermal synthesis to deposit p-hydroquinone over the GF- rGO material using same reaction conditions as last step. iv) Hydrothermal synthesis taking GF-HT and introducing in solution HNO3:H2O (1:1) for 12h at 80oC. v) Hydrothermal synthesis taking GFactivated or GF-HT and introducing a linear alcohol chain (ROH) as glycerol to deposit analogously to the step iii) for 12h at 80oC. 3.2.1 TiO2 synthesis An initial optimization synthesis is done placing 2 pieces of 4 cm2 graphite felt electrodes, which are previously treated for 10 min each side in an O2 plasma chamber, inside an hydrothermal reactor containing a water-hydrochloric acid (1:1) 44PDF Image | Redox Flow Batteries Vanadium to Earth Quinones
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