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a) 1μm GF-HT b) 2μm GF-TiO2 (NPs) 80o/0.1M 50nm c) GF-TiO2(SNRs) 100oC/0.1M 1μm 200 nm d) 200 nm GF-TiO2(MNRs) 10 μm Figure 6.2. – FESEM images of different titanium dioxide morphologies decorating the surface of the graphite felt a) GF-HT, b) GF-TiO2(NPs), c) GF-TiO2 (SNRs) and d) GF-TiO2 (MNRs).It is also shown a TEM image as the caption in b). Although the mentioned structural changes previously mentioned, there is no effective change in the XRD diffraction pattern (JCPDS no.: 21-1276) shown in Figure 6.3. In all cases, the peaks are related to titanium dioxide in its rutile form. It is also included the rutile unit cell, as well as, the crystallographic parameters related to it. The broad peak near 2θ = 250 and 430 in the spectrum of GF-P electrode is attributed to the crystallographic planes of (002) and (004) of the originally GF electrode. Additional diffraction peaks appears in the pattern of GF@TiO2 electrode at 27.40; 35.80 and 54.30; which are consistent with the rutile TiO2 (110), (101), and (211) crystalline planes, respectively. 85PDF Image | Redox Flow Batteries Vanadium to Earth Quinones
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