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Condens. Matter 2022, 7, 4 6 of 7 References Funding: This research was funded by JSPS KAKENHI grant number JP19K05519 and the U.S. De- partment of Energy (DOE), Office of Science, Basic Energy Sciences (Grant No. DE-FG02-07ER46352), and it also benefited from Northeastern University’s Advanced Scientific Computation Center (ASCC) and the NERSC Supercomputing Center through DOE (Grant No. DE-AC02-05CH11231). Data Availability Statement: The data that support the findings of this study are available upon reasonable requests from the corresponding author. Acknowledgments: K.S. was supported by JSPS KAKENHI Grant No. JP19K05519. Compton scatter- ing experiments were performed with the approval of JASRI (Proposal No. 2020A0648). The SQUID measurement was performed with the approval of Gunma University-Industry Collaboration and Intellectual Property Strategy Center (Proposal 2020). The work at Northeastern University was supported by the U.S. Department of Energy (DOE), Office of Science, Basic Energy Sciences (Grant No. DE-FG02-07ER46352), and the paper benefited from Northeastern University’s Advanced Scien- tific Computation Center (ASCC) and the NERSC Supercomputing Center through DOE (Grant No. DE-AC02-05CH11231). Conflicts of Interest: The authors declare no conflict of interest. 1. Assat, G.; Tarascon, J.M. Fundamental understanding and practical challenges of anionic redox activity in Li-ion batteries. Nat. Energy 2018, 3, 373–386. [CrossRef] 2. Okubo, M.; Yamada, A. Molecular orbital principles of oxygen-redox battery electrodes. ACS Appl. Mater. Interfaces 2017, 9, 36463–36472. [CrossRef] 3. Hafiz, H.; Suzuki, K.; Barbiellini, B.; Tsuji, N.; Yabuuchi, N.; Yamamoto, K.; Orikasa, Y.; Uchimoto, Y.; Sakurai, Y.; Sakurai, H.; et al. Tomographic reconstruction of oxygen orbitals in lithium-rich battery materials. Nature 2021, 594, 213–216. 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Hafiz, H.; Suzuki, K.; Barbiellini, B.; Orikasa, Y.; Callewaert, V.; Kaprzyk, S.; Itou, M.; Yamamoto, K.; Yamada, R.; Uchimoto, Y.; et al. Visualizing redox orbitals and their potentials in advanced lithium-ion battery materials using high- resolution X-ray Compton scattering. Sci. Adv. 2017, 3, e1700971. [CrossRef] [PubMed] 8. Suzuki, K.; Suzuki, S.; Otsuka, Y.; Tsuji, N.; Jalkanen, K.; Koskinen, J.; Hoshi, K.; Honkanen, A.P.; Hafiz, H.; Sakurai, Y.; et al. Redox oscillations in 18650-type lithium-ion cell revealed by in operando Compton scattering imaging. Appl. Phys. Lett. 2021, 118, 161902. [CrossRef] 9. Naylor, A.J.; Makkos, E.; Maibach, J.; Guerrini, N.; Sobkowiak, A.; Björklund, E.; Lozano, J.G.; Menon, A.S.; Younesi, R.; Roberts, M.R.; et al. Depth-dependent oxygen redox activity in lithium-rich layered oxide cathodes. J. Mater. Chem. A 2019, 7, 25355–25368. [CrossRef] 10. Li, M.; Liu, T.; Bi, X.; Chen, Z.; Amine, K.; Zhong, C.; Lu, J. 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