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Condens. Matter 2020, 5, 19 8 of 10 Department of Energy (DOE), Oce of Science, Basic Energy Sciences grant number DE-FG02-07ER46352, and benefited from Northeastern University’s Advanced Scientific Computation Center (ASCC) and the NERSC supercomputing center through DOE grant number DE-AC02-05CH11231. Acknowledgments: The HE-XRD experiments were performed with the approval of the Japan Synchrotron Radiation Research Institute (Proposal No.: 2016B1247). Conflicts of Interest: The authors declare no conflict of interest. References 1. Khilari, S.; Pandit, S.; Ghangrekar, M.M.; Das, D.; Pradhan, D. Graphene supported α-MnO2 nanotubes as a cathode catalyst for improved power generation and wastewater treatment in single-chambered microbial fuel cells. RSC Adv. 2013, 3, 7902. [CrossRef] 2. Post, J. Manganese oxide minerals: Crystal structures and economic and environmental significance. Proc. Natl. Acad. Sci. USA 1999, 96, 3447. [CrossRef] [PubMed] 3. Jin, K.; Chu, A.; Park, J.; Jeong, D.; Jerng, S.E.; Sim, U.; Jeong, H.-Y.; Lee, C.W.; Park, Y.-S.; Yang, K.D.; et al. Partially Oxidized Sub-10 nm MnO Nanocrystals with High Activity for Water Oxidation Catalysis. Sci. Rep. 2015, 5, 10279. [CrossRef] [PubMed] 4. Sinha, A.K.; Suzuki, K.; Takahara, M.; Azuma, H.; Nonaka, T.; Fukumoto, K. Mesostructured Manganese Oxide/Gold Nanoparticle Composites for Extensive Air Purification. Angew. Chem. Int. Ed. 2007, 46, 2891–2894. [CrossRef] 5. Huang, M.; Li, F.; Dong, F.; Zhang, Y.X.; Zhang, L.L. MnO2-based nanostructures for high-performance supercapacitors. J. Mater. Chem. A 2015, 3, 21380–21423. [CrossRef] 6. Hui, X.; Ying, S.M.; Xiaogan, L.; Guoliang, Y.; Chong, C. Porous manganese oxide generated from lithiation/delithiation with improved electrochemical oxidation for supercapacitors. J. Mater. Chem. 2011, 21, 15521–15526. [CrossRef] 7. Tang, N.; Tian, X.; Yang, C.; Pi, Z.; Han, Q. Facile synthesis of α-MnO2 nanorods for high-performance alkaline batteries. J. Phys. Chem. Solids 2010, 71, 258–262. [CrossRef] 8. Zhang, Y.; Steiner, J.D.; Uzodinma, J.; Walsh, J.; Zydlewski, B.; Lin, F.; Chen, Y.; Tang, J.; Pradhan, N.; Dai, Q. Thermally synthesized MnO nanoparticles for magnetic properties and lithium batteries. Mater. Res. Express 2019, 6, 25015. [CrossRef] 9. Tan, Y.; Meng, L.; Peng, Q.; Li, Y. One-dimensional single-crystalline Mn3O4nanostructures with tunable length and magnetic properties of Mn3O4 nanowires. Chem. Commun. 2011, 47, 1172–1174. [CrossRef] 10. Balamurugan, M.; Venkatesan, G.; Ramachandran, S.; Saravanan, S. Synthesis and Fabrication of Nanomaterials. Bloomsbury India 2015, 1, 31. 11. Cheng, F.F.; Zhao, J.; Song, W.; Li, C.; Ma, H.; Chen, J.; Shen, P. Facile Controlled Synthesis of MnO2 Nanostructures of Novel Shapes and Their Application in Batteries. Inorg. Chem. 2006, 45, 2038–2044. [CrossRef] [PubMed] 12. Tran, D.T.; Ozkaya, D. TEM-based Pair Distribution Function study of interatomic distances in C-supported Pt. J. Phys. Conf. Ser. 2017, 902, 12029. [CrossRef] 13. Guzzinati, G.; Altantzis, T.; Batuk, M.; De Backer, A.; Lumbeeck, G.; Samaee, V.; Batuk, D.; Idrissi, H.; Hadermann, J.; Van Aert, S.; et al. Recent Advances in Transmission Electron Microscopy for Materials Science at the EMAT Lab of the University of Antwerp. Materials 2018, 11, 1304. [CrossRef] [PubMed] 14. Midgley, P.A.; Weyland, M. 3D Electron Microscopy in the Physical Sciences: The Development of Z-Contrast and EFTEM Tomography. Ultramicroscopy 2003, 96, 413–431. [CrossRef] 15. Midgley, P.A.; Dunin-Borkowski, R.E. Electron Tomography and Holography in Materials Science. Nat. Mater. 2009, 8, 271–280. [CrossRef] 16. Ersen, O.; Florea, I.; Hirlimann, C.; Pham-Huu, C. Exploring Nanomaterials with 3D Electron Microscopy. Mater. Today 2015, 18, 395–408. [CrossRef] 17. Möbus, G.; Doole, R.C.; Inkson, B.J. Spectroscopic Electron Tomography. Ultramicroscopy 2003, 96, 433–451. [CrossRef] 18. Liakakos, N.; Gatel, C.; Blon, T.; Altantzis, T.; Lentijo-Mozo, S.; Garcia-Marcelot, C.; Lacroix, L.M.; Respaud, M.; Bals, S.; Van Tendeloo, G. Co-Fe Nanodumbbells: Synthesis, Structure, and Magnetic Properties. Nano Lett. 2014, 14, 2747–2754. [CrossRef]PDF Image | Structure of Manganese Oxide Nanoparticles Extracted via Pair Distribution Functions
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