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Methods for Chemical Analysis of Water and Wastes

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Methods for Chemical Analysis of Water and Wastes ( methods-chemical-analysis-water-and-wastes )

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3. Fuel Acetylene 4. OXIdant Air 5 Typeofflame OXldlzmg Notes 1. The mterference caused by alummum at concentratIOns greater than 2 mg/l IS masked by addition of lanthanum Sodmm, potassmm and calcIUm cause no mterference at concentratIOns less than 400 mg/l 2. The followmg lme may also be used 202 5 nm Relative SensItivity 25 3 To cover the range of magnesmm values normally observed m surface waters (0 1-20 mg/l), It IS suggested that either the 2025 nm lme be used or the burner head be rotated A 90' rotation of the burner head will produce approxtmately one-eighth the normal sensitivity 4 Data to be entered mto STORET must be reported as mg/l 5 The gravlmetnc method may also be used (Standard Methods, 14th Edition, p 221) Precision and Accuracy 1 In a smgle laboratory (EMSL), usmg dlsttlled water spiked at concentratIOns of 2 1 and 8 2 mg Mg/l the standard deviatIOns were ±O 1 and ±O 2, respectively Recovenes at both ofthese levels were 100% 242 1-2

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