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5 7 Potassmm IodIde (KI) Crystals, ACS Reagent Grade 58 SodIUm Acetate SolutIOn (275 gil) DIssolve 275 g sodmm acetate tnhydrate 5 9 5.10 511 5 12 5 13 5 14 5 15 5 16 5 17 5.18 5 19 520 521 522 523 (NaC2H 30 2-3H20 ) m dIstIlled water DIlute to 1 hter and filter SodIUm Chlonde (NaC!) Crystals, ACS Reagent Grade SodIUm Formate SolutIOn (500 gil) DIssolve 50 g sodmm formate (NaCH02) m hot dlsttlled water and dIlute to 100 ml SodIUm Molybdate SolutIOn (10 gil) DIssolve 1g sodIum molybdate (NazMo04-2HzO) m disttlled water and dtlute to 100 ml Sulfunc ACId SolutIOn (14) Slowly add 200 ml H2S04 (sp gr 1 84) to 800 ml ofdIstilled water Phenylarsme OXIde (00375N) Hach ChemIcal Co, or eq,Ulvalent StandardIze wIth 00375 N potassmm bllodate (5 19,523) Phenylarsme OXIde Workmg Standard (00075 N) Transfer 100 ml of commerCIally avallable 0 0375 N phenylarsme oXIde (5 13) to a 500 m1 volumetnc flask and dtlute to the mark wIth dlstdled water ThIs solutIOn should be prepared fresh dady Commercmll)PDF Image | Methods for Chemical Analysis of Water and Wastes
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