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sample hne When new tubIng is used, about 2 hours may be reqmred to obtaIn a stable baseltne ThIS two hour time penod may b~ necessary to remove the resIdual phenol from the tubIng 74 Place appropnate phenol standards In sampler In order of decreasIng concentratIon Complete loadIng pfsampler tray with unknown samples, USIng glass tubes NOTE 1: If samples have not been preserved as Instructed In (3 1), add 01 g CUS04 and 2dropsofconc H3P04to100mlofsample 75 SWItch sample hne from distdled water to sampler and begIn analysJs 8 CalculatIOn 8 1 Prepare standard Cllrve by plottIng peak heIghts of standards agamst concentratIon values Compute concentration of samples by comparIng sample peak heIghts wIth standards 9 PreCISIOn and Accuracy 91 In a smgle laboratory (EMSL), USIng sewage samples at concentrations of 3 8, 15, 43 and 89 ug/l, the standard devIations were ±0,5, ±O 6, ±O 6 and ±1.0 ug(l, respectively At concentrations of 73, 146, 299 and 447 tIg/1, the standard deviatIons were ±10, ±18, ±42and ±53ugfl,respectively 92 In a smgle laboratory (EMSL), usmg sewage samples at concentratIOns of 5 3 and 82 ug/l, the recovenes were 78% and 98% At concentratIons of 168 and 489 ug/l, the recovenes were 97% and 98%, respectively Bibliography 1 Techmcon AutoAnalyzer II Methodology, Industnal Method No 127-71W, AAII 2 Standard Methods for the EXamInation of Water and Wastewater, 14th EditIOn, p 574, Method 510 (1975) 3 Gales,ME andBooth,R.L,"Automated4AAPPhenoltcMethod",AWWA68,540(1976)PDF Image | Methods for Chemical Analysis of Water and Wastes
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