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observed and then collected after 30 min centrifugation at 3500 RPM. The concentration of Ti3C2Tx solution was measured by filtering specific amounts of colloidal solution through a polypropylene filter (3501 Coated PP, Celgard LLC, Charlotte, NC), followed by drying under vacuum at 70 °C overnight. 3.3.5.2 Preparation of MXene Microsupercapacitor PET sheets were cleaned with a soap solution to remove surface contamination followed by ultrasonication in isopropanol and DI water sequentially for 5 min each and then dried by blowing nitrogen (N2) gas. PET patterns were produced by utilizing direct laser machining using a CO2 Universal Laser cutter System (model: Professional laser system PLS 6.75, wavelength of 10.6 μm). The laser power and speed were set to 5% and 30%, respectively. The z-distance between the laser and the sample was 2 cm. AutoCAD technical drawing software was used to design the interdigital finger electrodes at each length of 8 mm, width of 1 mm, and spacing of 1 mm. The laser beam size was 100 μm. All of the laser experiments were performed under ambient conditions. MXene symmetric MSCs were fabricated by one-step spray-coating of a 4 μm Ti3C2Tx film directly onto the PET patterns as the active material. This spray-coated MXene electrode pattern was directly used for fabrication of collector-free microsupercapacitor device by casting the gel electrolyte. 3.3.5.3 Preparation of Gel Electrolyte The PVA/H3PO4 gel electrolyte was prepared as follows: 1 g of PVA (Mw = 89000- 98000, Sigma-Aldrich) was weighed and added into an RB flask containing 10 ml deionised water. The mixture was subsequently heated at 80 °C with constant stirring until 103PDF Image | HIGH PERFORMANCE TRIBOELECTRIC NANOGENERATOR AND ITS APPLICATIONS
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