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Figure 3. a) Schematic diagram showing the electron density transfer between Li2S4 and TiOx (yellow: S, green: Li, blue: Ti, red: O) (left) and vials of a Li2S4/tetrahydrofuran (THF) solution (1), and the same solution immediately upon contact (top) and after 1 h stirring contact (bottom) with graphite (2), VULCAN XC72 carbon (VC) (3), and Ti4O7 (4) (right). b) High-resolution XPS S 2p spectra of Li2S4, Li2S4 /Ti4O7, and Li2S4/VC. c) Distribution of sulfur species for Ti4O7/S-60 and VC carbon/S-60 cathodes upon discharge, as determined by operando XANES. d) DFT analysis of the adsorption of S species on Ti4O7 (1-20) and TiO2 (110) surfaces. a-c) Reproduced with permission.[58] Copyright 2014, Nature Publishing Group. d) Reproduced with permission.[59] Copyright 2014, American Chemical Society. 30PDF Image | Advances in Polar Materials for Lithium-Sulfur Batteries
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