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This thesis is structured in six chapters. Following this introduction, the materials and experimental methods are described in chapter 2. In addition to listing and de- scribing the experiments, the rationale behind each material or methodology choice is explained. Also, the design, setup, and optimization of the carbon coating furnace and the corresponding protocol is treated in this chapter. The results obtained are presented and discussed in chapter 3. Besides the successful demonstration of the use of carbon-coated lithium sulfide in a Li/S cell, valuable information on the mate- rial and cell level was collected and improvements to the performance and lifetime of Li/S cells are reported. Chapter 4 contains information on the modeling and model calibration methodology as well as a description of the Li/S model itself. Some the- oretical background including detailed explanations of the governing equations used for transport, thermodynamics, and electrochemistry is also part of this chapter. The proposed reaction mechanism is discussed along with possible routes of degradation. In chapter 5, the results of the simulations are presented, interpreted and discussed. Finally, the last chapter summarizes and interprets the achievements of this work and the impact on Li/S research. In the closing remarks, suggestions for future research are discussed alongside with progress in the field of electrochemical energy storage and its applications in general. Lengthy calculations, listings, and full bibliographic records can be found in the appendix. 16PDF Image | Lithium-Sulfur Battery: Design, Characterization, and Physically-based Modeling
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