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5 μm 0.5 μm (a) Li2S powder after high-energy ball-milling 5 μm 0.5 μm (b) Li2 S powder after ball-milling and carbon coating with ethylene at 700 °C 5 μm 0.5 μm (c) Li2 S powder after ball-milling and carbon coating with acetylene at 400–450 °C Figure 3.4: SEM micrographs of ball-milled and carbon-coated Li2S. Left column: 5 000× magnification, right: 50 000× magnification. Note how coating at elevated temperature causes agglomeration (b), whereas coating at lower temperatures (c) nearly preserves the particle size distribution of the ball- milled, uncoated material (a). For comparison, the pristine material is shown in Fig. 3.1a. 38PDF Image | Lithium-Sulfur Battery: Design, Characterization, and Physically-based Modeling
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