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Supercritical CO2 Mediated Incorporation of Sulfur into Carbon Matrix

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Supercritical CO2 Mediated Incorporation of Sulfur into Carbon Matrix ( supercritical-co2-mediated-incorporation-sulfur-into-carbon- )

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Paper Journal of Materials Chemistry A Fig. 5 (a) Digital photographs of AC@S and AC/S-155 soaked in electrolyte. (b) Comparison of the cycled AC@S and AC/S-155 cathodes soaked in DOL/DME solvent. (c) Digital photographs of the cycled separators of AC@S and AC/S-155 cells. In order to gain deep insight into the chemical composition and microstructure evolution of the AC@S electrode, SEM, TEM, XPS and BET tests of the cycled AC@S electrodes were further carried out. The morphology of the fresh AC@S elec- trodeisillustratedinFig.6aandb.ItwasfoundthatAC@Sand Super-P particles were uniformly dispersed on the surface of the View Article Online Fig. 6 (a, b, e and f) SEM images of the fresh and cycled AC@S electrodes. (c) TEM image of the cycled AC@S electrode. The inset is the HRTEM image of the cycled AC@S electrode. (d, g and h) STEM image and EDS mappings of the cycled AC@S electrode. (i and j) High-resolution S 2p and C 1s spectra of the cycled AC@S electrode. The cycled electrodes were charged in the delithiated state after 100 cycles. This journal is © The Royal Society of Chemistry 2017 J. Mater. Chem. A Published on 24 November 2017. Downloaded by University of Texas Libraries on 08/12/2017 20:16:36.

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Supercritical CO2 Mediated Incorporation of Sulfur into Carbon Matrix

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