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5.15: FE-SEM top-down (top) and cross sectional (bottom) of 100 vol. % ZnEO PRESS control sample. A dense film is observed.........................................................162 5.16: XRD of 50 vol. % ZnEO PRESS sample. XRD indicates polycrystalline zincite (ZnO) and ZnO2 are formed ..............................................................................163 5.17: XPS sputter depth profile (top) and survey scan (bottom) of 50 vol. % ZnEO PRESS sample. XPS indicates an atomic ratio of Zn:O::1:1 at the surface and a different atomic ratio of Zn:O::2:3, with no carbon contamination, in the bulk of the film...............................................................................................................164 A.1: Schematic of base plate for four point bend apparatus ........................................181 A.2: Top view of base plate for four point bend apparatus .........................................182 A.3: Side view of base plate for four point bend apparatus.........................................182 A.4: Bottom view of base plate for four point bend apparatus....................................182 A.5: Schematic (top and bottom view) of slider component for four point bend apparatus ............................................................................................................183 A.6: Schematic (side view) of slider component for four point bend apparatus .........184 A.7: Top view of slider component for four point bend apparatus..............................185 A.8: Side view of slider component for four point bend apparatus .............................185 A.9: Bottom view of slider component for four point bend apparatus ........................185 A.10: Top view of assemlbed four point bend apparatus ..............................................186 A.11: Side view of assemlbed four point bend apparatus..............................................186 A.12: Bottom view of assemlbed four point bend apparatus.........................................186 B.1: Schematic of top plate of heated stage designed for the cold wall reactor ..........188 B.2: Schematic of bottom plate of heated stage designed for the cold wall reactor....189 xxiiiPDF Image | Supercritical Fluid Deposition Of Thin Metal Films
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