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10.107/s0108270192009661(1993). 29 30 US 10,991,944B2 25Moon,S.etal.Encapsulatedmonoclinicsulfurforstable sulfurthatbestmatchesmonoclinicgammaphasesulfur cyclingofli-srechargeablebateries.AdvMater25, usingPDXLVersion2.8.4.0IntegratedPowderDifraction 6547-6553,doi:10.102/adma.201303166(2013). Software;monoclinicgammaphasesulfurorientedinthek 26Galacher,A.C.&Pinkerton,A.A.Aredeterminationof direction,andmonoclinicsulfurthatbestmatchesmono monclinicy-sulfur.ActaCrystalographicaSectionC 5clinicgammaphasesulfurorientedinthekdirectionusing CrystalStructureCommunications49,125-126,doi: PDXLVersion2.8.4.0IntegratedPowderDifractionSoft structureofmonoclinicsulfur.InorganicChemistry15, asubstratewithmonoclinicsulfurdepositedthereinthatis 19-201,doi:10.1021/ic50162a059(1976). 10 suitableforuseasacathodeinanelectrodeofacelor 28Jung,S.C.&Han,Y.-K.Monoclinicsulfurcathode bateryandaloadingofthemonoclinicphasesulfuronthe utilizingcarbonforhigh-performancelithium-sulfurbat- substrateisatleast0.5mg/cm2. teries.JournalofPowerSources325,495-50,doi: 13.Themethodofclaim1,whereinthedepositingstepis 10.1016/j.jpowsour.2016.06.057(2016). cariedoutinthesealedvapordepositionaparatusata 29Takahagi,T.& Ishitani,A.XPS studyonthesurface 15temperatureoffrom150°C.to210°C. structureofcarbonfibersusingchemicalmodificationand 14.Themethodofclaim1,whereinthedepositingstepis Clslineshapeanalysis.Carbon26,389-395,doi: cariedoutforaperiodof10to30hours. 10.1016/0008-6223(88)90231-x(1988). 15.Themethodofclaim1,whereinthecolingstepis 30Liang,X.etal.Ahighlyeficientpolysulfidemediatorfor cariedoutbyexposingthevapordepositionaparatusor lithium-sulfurbateries.Nat Commun 6,5682,doi:20thecathodetoatemperatureoffromabout-20°C.toabout ware . 27Templeton,L.K.,Templeton,D.H.&Zalkin,A.Crystal 12.Themethodofclaim1,whereinthemethodprovides 10.1038/ncomms6682(2015). What is claimed is: 25°C. 16.Themethodofclaim1,whereinthemonoclinicphase 1.Amethodofdepositingmonoclinicsulfuronasubstrate sulfurcomprisesaformofsulfurselectedfromthegroup ofaporousmaterial,comprisingstepsof: consistingofmonoclinicgammaphasesulfur;monoclinic depositingmonoclinicphasesulfurthatisstableata25sulfurthatbestmatchesPDFCardNo.:0-013-0141Quali temperaturebelow80°C.viavapordepositionontothe ty:BforRosickyite,monoclinicgammaphasesulfur,using substrateoftheporousmaterialinasealedvapor PDXLVersion2IntegratedPowderDifractionSoftware. deposition aparatus ata temperature suficientto 17.Themethodofclaim16,whereinthesubstrateis vaporizesulfurandforatimesuficienttoprovidethe non-conductiveandthemethodprovidesasubstratewith monoclinicphasesulfur,and 30monoclinicsulfurdepositedthereinthatissuitableforuseas colingthemonoclinicphasesulfurdepositedonthe acathodeinanelectrodeofacelorbateryandaloading substrateoftheporousmaterialtoatemperatureof ofthemonoclinicphasesulfuronthesubstrateisatleast0.5 0-50°C., mg/cm2andthedepositingstepiscariedoutinthesealed whereinthesubstrateispositionedinthevapordeposition vapordepositionaparatusatatemperatureoffrom150°C. aparatuswithagabbetwenasurfaceofaliquidsulfur35to210°C.foraperiodof10to30hours. reservoirandthesubstratesuchthatthesubstratedoesnot 18.Amethodofdepositingmonoclinicsulfuronasub comeintocontactwithliquidsulfurduringthevapordepo- strateofaporousmaterial,comprisingstepsof: sitionstep. depositingmonoclinicphasesulfurthatisstableata 2.Themethodofclaim1,whereinthemethodprovidesa temperaturebelow80°C.viavapordepositionontothe substratewithmonoclinicsulfurdepositedthereinthatis40 substrateoftheporousmaterialinasealedvapor suitableforuseasacathodeinanelectrodeofacelor deposition apparatus at a temperature suficient to bateryandaloadingofthemonoclinicphasesulfuronthe vaporizesulfurandforatimesuficienttoprovidethe substrateisatleast0.05mg/cm2. monoclinicphasesulfur,and 3.Themethodofclaim1,whereinthedepositingstepis colingthemonoclinicphasesulfurdepositedonthe cariedoutinthesealedvapordepositionaparatusata45 substrateoftheporousmaterialtoatemperatureof temperatureoffrom140°C.to350°C. 0-50°C., 4.Themethodofclaim1,whereinthedepositingstepis whereinthesubstrateisnon-conductive. cariedoutforaperiodofatleastabout1minute. 19.Amethodofdepositingmonoclinicsulfuronasub 5.Themethodofclaim1,whereinthecolingstepis strateofaporousmaterial,comprisingstepsof: cariedoutbyexposingthevapordepositionaparatusor50 depositingmonoclinicphasesulfurthatisstableata thecathodetoatemperatureoflesthan50°C. temperaturebelow80°C.viavapordepositionontothe 6.Themethodofclaim5,whereinthevapordeposition substrateoftheporousmaterialinasealedvapor aparatusiscoledimediatelyuponcompletionofthe depositionaparatusatatemperaturesuficientto depositingstep. 7.Themethodofclaim1,whereinthesubstrateofthe 5 monoclinicphasesulfur,and porousmaterialhasaporevolumeof10-95%afterdeposi- colingthemonoclinicphasesulfurdepositedonthe tionofthemonoclinicphasesulfuronthesubstrate. 8. The method of claim 1, wherein the substrate is substrateoftheporousmaterialtoatemperatureof 0-50° C., whereinthemethodprovidesasubstratewithmonoclinic conductive. 9.Themethodofclaim1,whereinthesubstratecomprises 60 sulfurdepositedthereinthatissuitableforuseasacathode inanelectrodeofacelorbateryandaloadingofthe 10.Themethodofclaim9,whereinthecarbonnanofibers monoclinicphasesulfuronthesubstrateisatleast0.5 ontowhichthemonoclinicphasesulfurisdepositedare mg/cm2andthedepositingstepiscariedoutinthesealed vapordepositionaparatusatatemperatureoffrom150°C. carbonnanofibers. fre-standingcarbonnanofibers. 1.Themethodofclaim1,whereinthemonoclinicphase65to210°C.foraperiodof10to30hours. sulfurcomprisesaformofsulfurselectedfromthegroup 20.Themethodofclaim19,whereinthecolingstepis consistingofmonoclinicgammaphasesulfur;monoclinic cariedoutbyexposingthevapordepositionaparatusor vaporizesulfurandforatimesuficienttoprovidethePDF Image | SYNTHESIS OF GAMMA MONOCLINIC SULFUR
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Sulfur Deposition on Carbon Nanofibers using Supercritical CO2 Sulfur Deposition on Carbon Nanofibers using Supercritical CO2. Gamma sulfur also known as mother of pearl sulfur and nacreous sulfur... More Info
CO2 Organic Rankine Cycle Experimenter Platform The supercritical CO2 phase change system is both a heat pump and organic rankine cycle which can be used for those purposes and as a supercritical extractor for advanced subcritical and supercritical extraction technology. Uses include producing nanoparticles, precious metal CO2 extraction, lithium battery recycling, and other applications... More Info
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