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Molecules 2019, 24, 182 8 of 41 reactions. DBU could capture and transfer protons; meanwhile, CuI activated the C≡C triple bond of Molecules 2019, 24, x FOR PEER REVIEW 8 of 42 propargylic amine. Similarly, CuI/[DBUH][TFE] (9, Scheme 6c) system also afforded 2-oxazolidinones inoutpsrtoapnadrignyglicyiealmdsinuen.deSirmmilailrdlyc,onCduiIt/i[oDnBsU[H48][]T.FME]ore(o9,verS,cHheemaend6c)o-wsyosrtkemerseaxlspoloiatfefdordaesderiesof metal2-s-ouxbasztoitliudtiendonpeosliynooxuotmstaentadliantge y(PieOldMs u)-nbdaesredmiIlLdscioncdluitidoinsg[4C8u].(MII)o,rCeov(eIIr),,HFe(aIIn)d, Ncoi-(wIIo),rkZenr(sII) and exploited a series of metanl-substituted polyoxometalate (POM)-based ILs including Cu(II), Co(II), Mn(II) [49]. Among them, [( C7H15)4N]6[α-SiW11O39Cu] (10, Scheme 6c) displayed higher catalytic Fe(II), Ni(II), Zn(II) and Mn(II) [49]. Among them, [(nC7H15)4N]6[α-SiW11O39Cu] (10, Scheme 6c) activity than that of other metal-substituted POM-based ILs. It was mainly ascribed to simultaneous displayed higher catalytic activity than that of other metal-substituted POM-based ILs. It was activation of propargylic amines and CO2 by the single-component catalyst. Notably, this procedure mainly ascribed to simultaneous activation of propargylic amines and CO2 by the single-component featured as environmentally benign and low energy-input manner. catalyst. Notably, this procedure featured as environmentally benign and low energy-input manner. Scheme 6. A summary of coinage metals catalysts in carboxylative cyclization of propargylic amines with CO2.PDF Image | Catalytic Conversion of Carbon Dioxide through C-N Bond
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