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1CO2 UTILIZATION ECCO2 Fig. 20: SFC-DEMS CELL: the products are fed into the MS via a suction tube The probe (i.e. the working electrode) is located on an XYZ positioning table, while the reference and counter electrodes are housed within the flow cell itself. Figure 1 depicts a flow cell with a channel diameter of, in this case, 1 mm; diameters ranging from 200 μm to 3 mm are possible. The probe can be moved underneath the cell in any direction and can also be brought in- to contact with the cell. In the latter case, the electrolyte has contact with the probe via a small orifice at the tip of the v-shaped flow path. Electrolyte solution is continuously pumped through the cell even when the probe is being moved into a new position. In the case of a homogeneously structured working electrode, the benefits of the SFC over more conventional meth- ods are the high level of reproducibility that can be achieved and the speed with which measurements can be conducted. If the working electrode has a graded composition, the speed with which measurements can be performed and the resolution attainable is far superior to that achievable with standard methods of examination. When a graded working electrode is used, chang- ing the location on the electrode automatically changes the composition, and the resolution achievable is then only dependent on the size of the cell orifice. Using a flow cell also means that online analyses of dissolution and 56PDF Image | Chemical Processes and Use of CO2
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