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DMEEXCO2 FUNDED PROJECTS syngas generation and DME synthesis stages. The results of that work package were used by the project partners to jointly agree milestones and perfor- mance criteria for subsequent catalyst development work. In addition, the conceptual engineering phase for the lab-scale plant and the miniplant (technical centre) was also initiated at this time. In the second year of the project, the process design work focused on workup procedures for the DME product and on evaluating a number of different recycling options. A differential reactor for the experimental kinetic studies was made available at this stage and the planning, procurement and con- struction of the miniplant in the technical centre was completed. During year two of the project and before the two cost-intensive miniplants were commissioned at BASF and Linde, the project partners all gave positive as- sessments of the agreed milestones regarding the energy efficiency of the process, CO2 emissions savings and catalyst performance. In the third year of the project, the knowledge acquired thus far was used to optimise and validate the process with the help of detailed process simula- tions. A series of experiments were conducted in the differential reactor in order to describe the kinetics of the catalyst system. During a number of the experimental campaigns at Linde the miniplant was operated continuously. While project work was being undertaken at the two industrial partners, the research team led by Professor Ferdi Schüth at the Max Planck Institute for Coal Research examined the deactivation mechanism and tested a number of alternative catalyst recipes. The results of the mechanistic studies were used to fine-tune the catalyst recipe towards the latter end of the project. Another work package that was carried out at the same time concerned benchmarking the fixed bed reactor design preferred by the project partners against the slurry-type reactor that has been the only type of reactor to be described so far in the scientific literature. A new test plant was therefore Fig. 24: Pilot reactor setups at BASF (left) and Linde (right) 71PDF Image | Chemical Processes and Use of CO2
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