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1CO2 UTILIZATION FFPAG Fig. 30: Test production facilities (lab and pilot scale) for the high-temperature pyrolysis of natural gas; (2014 and 2015) 1.10.3 Results The planned trial production facilities, with sizes ranging from lab scale to semi-pilot scale, have all been built and are currently in operation. Experi- mental studies are being carried out in the areas: reaction kinetics, heating technology, heat integration, materials selection and equipment structure and design. Parallel studies aimed at modelling the underlying reactive sys- tem (published, for example, in [4]) and at simulating the overall technolog- ical process have yielded important information for the design of the pro- posed pilot plant. New information on residence time behaviour, on the required material stability and durability and on measures that can be used to suppress the back reaction go far beyond what has been understood so far and provide an excellent basis for the design of the pyrolysis reactor. In order to ensure that the carbon product is suitable for subsequent indus- trial applications, a specially designed trial batch production facility will be built to manufacture quantities at the semi-pilot scale. The trial batch production facility shown in Figure 30 will be commissioned in 2016. The test batches will be used to examine a range of approaches to solid prod- uct workup and processing and to carry out application tests, e.g. coking/ carbonisation experiments. Operating the trial batch production facility will also yield important information about the relationships between key op- erational parameters such as temperature and residence time and product Fig. 31: Trial batch facility for the production of batches of carbon for testing; (2016) 84PDF Image | Chemical Processes and Use of CO2
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