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3 ENERGY-EFFICIENT PROCESSES HY-SILP Fig. 102: SILP pore loading before and during the reaction; Progress of reaction as a function of different carrier materials used in the SILP system [2] sion the overall process. The deactivated SILP systems were analysed and recycling concepts for recovering the transition metals from the deactivated SILP catalysts were developed. 3.11.3 Results As a result of the HY-SILP project, it was possible to identify the performan- ce-limiting factors in SILP catalysis. The main factors are the available phase boundary surface as a function of loading and IL, and the pore size distribu- tion within the SILP carrier material. The extent of pore loading in the SILP system and its effect on the start-up behaviour of the hydroformylation reaction are shown in Figure 102 [2–4]. In the prepared SILP system, the transition metal catalyst is physisorbed on the pore surface prior to reaction. Under the prevailing reaction conditions the aldehydes generated can form high concentrations of aldol as a result Acid cat. Fig. 103: Example of a secondary reaction in which the aldehydes initially formed react further to produce higher-boiling aldol condensates 258PDF Image | Chemical Processes and Use of CO2
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