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C 2020, 6, 34 8 of 21 C 2020, 6, x FOR PEER REVIEW 8 of 21 Scheme 4. Proposal mechanism for 4-nitrobenzene electrochemical reduction under inert Scheme 4. Proposal mechanism for 4-nitrobenzene electrochemical reduction under inert atmosphere. 3.2.ElectrochemicalBehaviourofNitro-CompoundsunderCO Atmposphere 3.2. Electrochemical Behaviour of Nitro-Compounds under C2O2 Atmposphere atmosphere. CompoundsC1o-m4psohuonwdss1a-4clsehaorwlys daiffcleraerlnytdbieffheraevnitobuerhwavhioeunr twhheecnytchleiccvyoclliacmvomlaomgmraomgrasmasrearecorded recorded under CO2 atmosphere, although they show the same general trend in aprotic solvent and under CO2 atmosphere, although they show the same general trend in aprotic solvent and ionic liquid. ionic liquid. Also the follow same tendency in C, Ag and Cu working electrodes; there was a rising Also the follow same tendency in C, Ag and Cu working electrodes; there was a rising in current value in current value of the reduction peak and its reversibility was lost (Figure 3), which indicates that p- of the reduction peak and its reversibility was lost (Figure 3), which indicates that p-nitrocompounds nitrocompounds 1-4 follow a demeanor of an organic mediator for CO2 indirect reduction through a 1-4 follow a dhoemoegaeneoorusocfaatanlyoticrgparonciecssm(Sechdeimateo5r).for CO2 indirect reduction through a homogeneous catalytic process (Scheme 5). C 2020, 6, x FOR PEER REVIEW 9 of 21 Figure 3. Cyclic voltammetry of 10 mM p-nitro compounds 1-4 with Ag (black line), Cu (red line) and Figure 3. Cyclic voltammetry of 10 mM p-nitro compounds 1-4 with Ag (black line), Cu (red line) and −1 C(bluelinCe)(,blunedlineer),CuOndeartCmOo −1 Eq. 10 XX + 1e- solution of 3 mL EMIM TFSI (right). solution of 3 mL EMIM TFSI (right). O2N X: CH3, F, Cl, I O2N T(BleAft)BanFd (left)and saptmhoesrpeh.erSec.aSncanrartaete::0.5V·s·s.S.olSuotilountoiofnDMofF/D0.1MFT/0B.A1MBF4 24 2 Electrochemical reductionPDF Image | Electrochemical Tuning of CO2 Reactivity in Ionic Liquids
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