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Materials 2021, 14, 1786 Materials 2021, 14, 1786 13 of 19 13 of 20 3.3. Crystalline and Morphology Analysis Scanning electron microscopy (SEM) characterization was performed for all Tb- based CPs, and the results are summarized in Figure 7, including the respective EDX spec- 3.3. Crystalline and Morphology Analysis tra for each one of the materials. This analysis is important to evaluate the approximate Scanning electron microscopy (SEM) characterization was performed for all Tb-based size and morphology of the prepared CP materials and may also help in the assessment CPs, and the results are summarized in Figure 7, including the respective EDX spectra of the presence of organic/inorganic contaminants or other crystalline phases (EDX anal- for each one of the materials. This analysis is important to evaluate the approximate size ysis). and morphology of the prepared CP materials and may also help in the assessment of the presence of organic/inorganic contaminants or other crystalline phases (EDX analysis). (a) (b) (c) (d) Figure 7. SEM images and respective EDX spectra for TbCP1 prepared by MWAS (a) and HT (b), TbCP2 (c) and TbCP3 Figure 7. SEM images and respective EDX spectra for TbCP1 prepared by MWAS (a) and HT (b), TbCP2 (c) and TbCP3 (d). (d). SEM analysis of TbCP1 reveals that the material prepared by HT is more disperse SEM analysis of TbCP1 reveals that the material prepared by HT is more disperse and morphologically more homogeneous than the one prepared by MWAS, that shows and morphologically more homogeneous than the one prepared by MWAS, that shows agglomerates of long needles (Figure 7a,b). Most probably, these differences may be asgsgolcoimaterdawtesithofalodnisgtinecetdclreyss(tFailgliuzaretio7an,bp)r.oMceosst, pfarsotbearbinlyt,htheecsaesedioffeMreWncAesSmcoanysbideearsinsog- tchiatetdhwe ictohoalindgisttiankcetscraybsotaultliz2a0timoninprinocsetesas,dfaosftetrheinstehveecraslehofuMrsWofAtShceoHnsTidseyrintghethsiast (tphreocmootliendgbtyaktehseadbioffuetre2n0cme in itnhsetereaadcotifotnhveessesveelrsa, lghlaosusrfsoorfMthWeAHSTasnydntTheeflsoisn(/psrtoaminoletessd rbeyactthoerdfiofrfeHreTn)c.eIin gtheenerrealc,tiaonfavsetesrseclos,oglilnagsspforormMoWteAs SthaendprTeepfalorant/isotnainolfesmsarteearcitaolrs fofr lHowT)e.rIncrgyesntaelrlianl,itayfanstderlocwooelrincgonpvreormsiotnesinthtoe tphrepdaersairteiodnCoPf.mDaetsepritaelsthoifsldowisseirmcirlyasrtiatyllin- tihtyeamnodrlpohwoelrogcoynovfetrhsieonTbinCtoP1thoebdtaeisnireedbCyPM.DWesApSiteanthdisHdTissiymnitlhaersitiys,itnhtehpeomwodrpehroXlRogDy aonfathlyesTisbcCoPn1firombteadintehdatbythMeWcryAsStaallnindeHmTastyenritahlessiso,ltahtedpobwydtehreXtRwDoamneatlhyosidsscohnavfiermtheed stahmatethseolcirdy-staltleinsetrmucatueriealasnidsoiltatlaedrgbeylythcoertrwesopmonedthsotdosthavteptrheedsicatmede sfroolimd-sthtaetesisntrgulec- ctruyrsetalndaitalasirmgeulylactiornre(sFpiognudres 8to). tHhaotwpervederi,ctehde forbosmertvhaetisoingolfe-acrfyewstaalddaittaiosnimaluplaetaikosn relatively to simulated, points to the residual presence of some additional crystalline phase (Figure 8). However, the observation of a few additional peaks relatively to simulated, or compound. Most probably, these additional peaks can correspond to some residualPDF Image | Green Chemistry with Supercritical CO2 and Enzymes
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