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Coatings 2021, 11, 854 11 of 13 References Supplementary Materials: The following are available online at https://www.mdpi.com/article/ 10.3390/coatings11070854/s1. Figure S1: SEM images of products under different sodium hydroxide addition conditions, Figure S2: (a) Raman diagram of products with different sodium hydroxide addition levels, (b) Centrifugation results of products with addition volume of 16 mmol, Figure S3: (a) FTIR spectrum of MIL-121 and (b) Raman spectrum of MIL-121, Figure S4: Size distribution of (a) MIL-121-80 ◦C (hydrothermal method from Section 2.4), (b) MIL-121-90 ◦C (hydrothermal method from Section 2.4), (c) MIL-121-100 ◦C (hydrothermal method from Section 2.4), (d) MIL-121-80 ◦C scale 100 mL (Cooling crystallization method from Section 2.6), Figure S5: Raman spectra of (a) Al(NO3)3·9H2O, (b) H4BTEC, (c) pyromellitic acid hydrate, (d) MIL-121, Figure S6: (a) PXRD pattern of MIL-121-(1 atm, 80 ◦C), EasyMax product, (b) FTIR spectrum of MIL-121-(1 atm, 80 ◦C), EasyMax product and (c) Raman spectrum of MIL-121-(1 atm, 80 ◦C), EasyMax product, Table S1: Peaks location of PXRD pattern and the crystal indices of MIL-121 [2], MIL-121-80 ◦C NaOH 4 mmol, Table S2: The particle size distribution of MIL-121 under different temperature, Table S3: Preparation method and preparation time of partial aluminum-based MOF, Table S4: TGA mass loss of N-MIL-121 crystals synthesized under different conditions, Table S5: The adsorption performance test data of MIL-121 after polymerization obtained under different experimental condition. Author Contributions: Writing—review and editing, investigation and validation, Q.W., S.S. and B.S.; formal analysis and writing—original draft preparation, F.W.; writing—review and editing, and su- pervision, L.Z. and X.Z. All authors have read and agreed to the published version of the manuscript. Funding: Natural Science Foundation of Tianjin Municipality (18JCYBJC21200). Institutional Review Board Statement: Not applicable. Informed Consent Statement: Not applicable. Data Availability Statement: Data is contained within Supplementary Materials. The data presented in this study are available in Supplementary Materials. Acknowledgments: Thanks to the College of Chemical Engineering and Materials Science for pro- viding instruments and experimental materials. Conflicts of Interest: The authors declare no conflict of interest. 1. Swain, B. Recovery and recycling of lithium: A review. Sep. Purif. Technol. 2017, 172, 388–403. [CrossRef] 2. Jiang, H.; Yang, Y.; Sun, S.; Yu, J. Adsorption of lithium ions on lithium-aluminum hydroxides: Equilibrium and kinetics. Can. J. Chem. Eng. 2020, 98, 544–555. [CrossRef] 3. Chung, K.; Lee, J.; Kim, W.; Kim, S.; Cho, K. Inorganic adsorbent containing polymeric membrane reservoir for the recovery of lithium from seawater. J. Membr. Sci. 2008, 325, 503–508. [CrossRef] 4. Zhang, Y.; Hu, Y.; Wang, L.; Sun, W. Systematic review of lithium extraction from salt-lake brines via precipitation approaches. Miner. Eng. 2019, 139, 105868. [CrossRef] 5. Zhao, X.; Yang, H.; Wang, Y.; Sha, Z. Review on the electrochemical extraction of lithium from seawater/brine. J. Electroanal. Chem. 2019, 850, 113389. [CrossRef] 6. Zhao, X.; Li, G.; Feng, M.; Wang, Y. Semi-continuous electrochemical extraction of lithium from brine using CF-NMMO/AC asymmetric hybrid capacitors. Electrochim. Acta 2019, 331, 135285. [CrossRef] 7. Zhao, X.; Jiao, Y.; Xue, P.; Feng, M.; Sha, Z. Efficiently lithium extraction from brine by using three-dimensional (3D) nanostructured hybrid inorganic-gel framework electrode. ACS Sustain. Chem. Eng. 2020, 8, 4827–4837. [CrossRef] 8. Zhao, X.; Feng, M.; Jiao, Y.; Zhang, Y.; Wang, Y.; Sha, Z. Lithium extraction from brine in an ionic selective desalination battery. Desalination 2020, 481, 114360. [CrossRef] 9. Hu, S.; Sun, Y.; Pu, M.; Yun, R.; Xiang, X. Determination of boundary conditions for highly efficient separation of magnesium and lithium from salt lake brine by reaction-coupled separation technology. Sep. Purif. Technol. 2019, 229, 115813. [CrossRef] 10. Liu, Y.T.; Chen, T.-Y.; Wang, M.K.; Huang, P.M.; Chiang, P.-N.; Lee, J.F. Mechanistic study of arsenate adsorption on lithium/aluminum layered double hydroxide. Appl. Clay Sci. 2010, 48, 485–491. [CrossRef] 11. Shi, C.; Jing, Y.; Jia, Y. Solvent extraction of lithium ions by tri-n-butyl phosphate using a room temperature ionic liquid. J. Mol. Liq. 2016, 215, 640–646. [CrossRef] 12. Wei, X.; Liang, S.; Zhou, Z.; Qin, W.; Fei, W. Extraction of lithium from salt lake brine containing borate anion and high concentration of magnesium. Hydrometallurgy 2016, 166, 9–15. 13. Tian, L.; Wei, M.; Mei, H. Adsorption behavior of Li+ onto nano-lithium ion sieve from hybrid magnesium/lithium manganese oxide-sciencedirect. CEJ 2010, 156, 134–140.PDF Image | Small Particles for Lithium Adsorption from Brine
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Product and Development Focus for Infinity Turbine
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