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Figure 6-4. Photograph and diagram of ceramic cone-type point electrode used in the electrochemistry tests....................................................................................................................................183 Figure 6-5. X-ray diffractograms of some of the synthesized materials. ............................................187 Figure 6-6. Electrical conductivity versus temperature or pO2 for (a) SM, (b,c) SVM, (d) LM, and (e,f) STM. .......................................................................................................................................................188 Figure 6-7. Electrical conductivity measurements of the air-sintered Sr2MgMoO6 sample ............ 189 Figure 6-8. Electrical conductivity measurements of the reducing-sintered Sr2MgMoO6 sample SMM_2. ..........................................................................................................................................................190 Figure 6-9. Electrical conductivity measurements made on 3 different SNM samples....................191 Figure 6-10. Long-term electrical conductivity measurements of air-sintered samples (a) SNM_4, tested at 800 °C in 10-23 atm O2, and (b) SCM, tested at 800 °C in 10-24 atm O2 ...............................192 Figure 6-11. Electricity conductivity of Sr2FeMoO6 in dry 9% H2/Ar...............................................193 Figure 6-12. SEM micrograph of the SNM_2 polished surface after the conductivity test.............197 Figure 6-13. SEM micrograph of the SNM_2 polished surface after the conductivity test.............197 Figure 6-14. SEM micrograph of the SNM_2 polished surface after the conductivity test, with the backscatter detector. ..................................................................................................................................... 198 Figure 6-15. SEM micrograph of the SNM_2 polished surface after the conductivity test.............198 Figure 6-16. SEM micrograph of the SNM_3 polished surface after the conductivity test. SNM_3 had been exposed to a more reducing atmosphere and for a longer time. .......................................... 199 Figure 6-17. SEM micrograph of the SNM_4 polished surface after the conductivity test.............199 Figure 6-18. SEM micrograph of the polished surface of another SNM sample that had not been used in a conductivity test but only heat treated in a reducing atmosphere. .......................................200 Figure 6-19. EDX spectral map of the grain boundary particles of sample SNM_2. ....................... 200 Figure 6-20. SEM micrograph of an unpolished surface of one of the reduced SNM samples. ....201 Figure 6-21. SEM micrograph of an unpolished surface of one of the reduced SNM samples......201 Figure 6-22. SEM micrograph of an unpolished surface of one of the reduced SNM samples. ....202 Figure 6-23. SEM micrograph of an unpolished surface of one of the reduced SNM samples. ....202 Figure 6-24. X-ray diffractograms of an SNM sample that was subjected to reduction and re- oxidation. ........................................................................................................................................................ 203 Figure 6-25. Continuation of the 300-h SNM conductivity test shown in Figure 6-10a, with pO2 variations include oxidation in air and re-reduction in dry 9% H2/Ar.................................................203 viiiPDF Image | Electrolysis of CO2 and H2O
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