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Figure 6-26. Contact area of the tip of an SFM cone type electrode that had been in contact with the smooth polished YSZ surface ..............................................................................................................204 Figure 6-27. Example impedance spectra measured at OCV at 850 °C on (a) one of the STM electrodes, and (b) one of the SFM electrodes ......................................................................................... 205 Figure 6-28. Relative electrochemical performance of the tested materials, in terms of the LSRP at OCV in 3% H2O/H2, 50% H2O/H2, and 50% CO2/CO. ....................................................................205 Figure 6-29. Impedance spectra measured at OCV on the non-pre-reduced SNM electrode in 3% H2O/H2 at 850 °C ........................................................................................................................................206 Figure 6-30. Potential sweep on the SVM electrode, at 2 mV/s at 850 °C in 50% H2O/H2 .........209 Figure 6-31. (a) Activation factors of LSRP measured under bias relative to OCV LSRP and (b) TPB-length-specific currents, obtained at anodic (+200 mV) and cathodic (–200 mV) overpotentials at 850 °C in 50% H2O/H2...........................................................................................................................209 Figure 6-32. Electrochemistry measurements made on the STN-CGO cone-shaped electrode contacting the polished YSZ surface: (a) Impedance spectra measured at OCV, (b) Potential sweeps measured at 2 mV/s. ....................................................................................................................................210 Figure 8-1. Impedance spectra measured on the Ni electrode after oxidation at 1000 °C in 50 % H2O/H2 under (a) anodic bias and (b) cathodic bias .............................................................................. 222 Figure 8-2. Impedance spectra measured on the Ni electrode after oxidation at 850 °C in 50 H2O/H2 under (a) anodic bias and (b) cathodic bias .............................................................................. 222 Figure 8-3. Impedance spectra measured on the Ni electrode after oxidation at 850 °C in 50 CO2/CO under (a) anodic bias and (b) cathodic bias ............................................................................. 223 ixPDF Image | Electrolysis of CO2 and H2O
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