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Chapter 5. Aspects of Metal-YSZ Electrode Kinetics 121 similarly high reproducibility between electrodes for TPBL-normalized impedance measure- ments. Ni Pd Pt Cu Ag Au Figure 5-6. SEM micrographs of the flattened contact areas of representative wires of each metal. The scale bar shown in each is 100 microns. The smooth electropolished Ni wires are not shown. Large pieces of YSZ electrolyte were sometimes attached (not shown). The 3 lowest melting point metals (Cu, Ag, Au) crept the most, resulting in the largest contact areas. Some Pd wires such as the one shown formed a crack when bent, which did not heal, resulting in 2 separated contact areas. The bulb-tipped electrodes (not shown) formed a more circular interface rather than the elliptical shape seen here for Ni, Pd, and Pt. Table 5-2. Examples of the normalization process. The shaded columns are measurements. The two factors fc,area and fc,per are obtained by dividing ASEM/AN and xSEM/ respectively. 2.30 1.51 2.13 1.37 2.07 1.64 2.30 1.42 1.73 1.39 1.95 2.59 1.88 2.53 Final RS (Ω) Final T (°C) rN AN (mm) (mm2) ASEM (mm2) fc,area (mm) xSEM (mm) 235 849 0.181 1.84 249 849 0.149 1.91 206 849 0.213 2.02 249 849 0.161 1.81 189 854 0.153 3.30 Elec- trode Ni-1 Ni-2 Ni-3 Ni-4 Ni-5 Cu-1 107 Cu-2 108 854 854 0.158 0.079 0.149 0.070 0.181 0.103 0.149 0.070 0.168 0.089 0.296 0.275 0.294 0.272 0.536 0.510 fc,per 1.22 1.39 1.24 1.27 2.38 2.98 1.15 2.94 1.16PDF Image | Electrolysis of CO2 and H2O
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