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Chapter 5. Aspects of Metal-YSZ Electrode Kinetics 133 the mobilization of impurities at the TPB (e.g. the abovementioned Si(OH)4 reaction) could contribute to the activation and oscillations. Figure 5-13. Potential sweeps of H2 oxidation (positive voltage) and H2O reduction (negative voltage) at Ni/YSZ at different temperatures and gas compositions, measured in the order listed in the legend. The current is normalized to the TPBL. The OCV corresponds to a different potential versus air (a different pO2) for each curve, as labeled in the legend. The shading of the points behind the curves changes from black to light gray with time. The sweep rate for each was 1 mV/s. Possible linear regions in the log current plot are marked with dashed lines. Note: the noise near OCV for the black curve is measurement noise due to the low currents measured – unlike the oscillations seen at the higher voltages.PDF Image | Electrolysis of CO2 and H2O
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