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Appendix 2. Summary of Experiments Conducted 224 9. Appendix 2. Summary of Experiments Conducted Much more work went into these studies than has been presented, especially for the extensive metal and ceramic electrode materials studies of Chapter 5 and 6. A number of additional ceramic materials were prepared, and others were attempted but the desired phase could not be obtained. The additional materials that were prepared and have not been included were left out simply because either they did not exhibit especially interesting properties or no new information was obtained that had not been reported in literature. In these cases the materials were abandoned, but the work done was still useful as it contributed to understanding other related materials. For the materials that were included in these studies, a number of tests were most often conducted in order to properly understand the material and obtain the desired results (and to repeat experiments when things went wrong with the test set-ups). The experimental process was iterative, with each new result feeding back into the planning of the next tests. By the end, an optimized set of procedures was obtained, from the synthesis of the desired phase to the preparation and testing of the electrodes with an optimal sequence of conditions, with phase and microstructural checks at each stage. These methods took advantage of automated test set- ups, especially for the conductivity and electrochemistry tests (4 cells were tested simultaneously in the electrochemistry set-up), and produced almost more results than could be properly analyzed. In the end, it was necessary to automate the data analysis as well – automated data collection necessitates automated data processing. A collection of interactive Python scripts were written, as mentioned in the Acknowledgements at the start of this thesis. Creating these tools required a large up-front time investment which saved an enormous amount of time later. The most rewarding part of the analysis part of the work was when the tools became useable, enabling a transition to a productive and enjoyable workflow in which it was exciting (rather than unbearable) to pour through the data, graphically. Without this effort, if the measurements could only be analyzed one at a time, it seems rather certain that the work would have been impossiblei, evident in the statistics given in Table 9-1. i That is not to say that this is always the case – a very clearly planned set of experiments can be conducted with a minimal amount of measurements or carefully selected measurements, but this often requires knowing a lot beforehand about how the sample will behave. It most likely depends on the degree to which the work is exploratory in nature.PDF Image | Electrolysis of CO2 and H2O
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