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Appendix 2. Summary of Experiments Conducted 225 Table 9-1. Summary of experiments conducted. Full-cell testa (Chapter 4) Number of cells tested Number of electrochemistry measurementsb Metals (Chapter 5) Number of electrodes tested Number of electrochemistry measurementsb Ceramics (Chapter 6) Number of powder samples Number of dense sintered samples Number of conductivity samples tested Number of electrodes testedc Number of electrochemistry measurementsb Number of X-ray diffractograms Number of SEM images taken 7 1314 26 6849 367 211 41 64 4852 344 1103 a Including the electrolysis test described in Chapter 4 and a few additional related tests (preliminary button-cell tests at Columbia and two additional full-cell tests conducted in cooperation with Sune Ebbesen at Risø). b The electrochemistry measurements included impedance spectroscopy (accounting for the vast majority), polarization curves, and chronoamperometry. Impedance spectra were measured almost continually during many of the metal and ceramic point electrode tests to monitor the electrodes and determine when steady states were reached. These monitoring measurements account for a large fraction of the total number of measurements. c As mentioned in section 6.2, a side project was carried out to compare different simplified electrode geometries, which required a number of different electrodes made from the same material just for that purpose.PDF Image | Electrolysis of CO2 and H2O
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