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Catalysts 2021, 11, x FOR PEER REVIEW Catalysts 2021, 11, 482 5 of 19 Figure 2. CV responses for electrodes with Cu-06 catalyst (a) and Linear Sweep Voltammetry (LSV) Figure 2. CV responses for electrodes with Cu-06 catalyst (a) and Linear Sweep Voltammetry (LSV) responses un responses under CO flow of electrodes with Cu-06, CuZ-06-01, and CuZA-06-03-01 catalysts (b). flow of electrodes with Cu-06, C2uZ-06-01, and CuZA-06-03-01 catalysts (b). The catalyst loading was ⁓4 mg c The catalyst loading was ~4 mg cm−2, the Catalyst/Nafion ratio was 70/30 in all cases, and the tests Catalyst/Nafion ratio was 70/30 in all cases, and the tests were carried out in 1 M KHCO3 aqueous electrolyte. were carried out in 1 M KHCO3 aqueous electrolyte. Figure 2b displays the Linear Sweep Voltammetry (LSV) results under C For comparison, a blank test was performed to have a reference for the evaluation all the studied Cu-based electrocatalysts. A lower onset potential is noticed f of the products that may be generated from the only carbon support. Thus, the electro- lysts containing ZnO and Al2O3, which confirms the role of these metal oxides chemical behaviour of a carbon paper with a deposited ink without catalyst nanoparticles ing catalytic activity. At higher applied potentials, the catalytic activity does is described in Section S7 of the SI. In this case, the ink was constituted only by Vulcan to increase, although the CuZ-06-03 shows a current density value that is Carbon, Nafion solution, and isopropyl alcohol. This blank electrode generates current density valuesgrienatheer tChVanththateaortehecormtwpoarcaabtlaelytosttsh,ethoenmesaoxbimseurvmedapwpiltihedthpeoctaetnatliyasleodf −2 V v GDEs, under bTohteh mNaxainmduCmOacfltoivwitcyoonbdsiteirovnesd(sienetFhiegsuerecaSs6eisn(trheeduSIc)t;ihoonwcuevrreer,nutsndPDF Image | Gas Diffusion Electrode Systems for the Electro CO2 Conversion
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