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Materials 2021, 14, 1617 19 of 20 Figure A5. FE-SEM images of cross-linked diblock A150G4S-10 membrane (magnification 50,000×). Figure A6. FE-SEM images of cross-linked diblock A150G4S-10 membrane (magnification Figure A6. FE-SEM images of cross-linked diblock A150G4S-10 membrane (magnification 100,000×). 100,000×). References References 1. 2. 1. 2. 3. Erdogan, T.; Unveren, E.E.; Inan, T.Y.; Birkan, B. Well-defined block copolymer ionomers and their blend membranes for proton exchange membrane fuel cell. J. Membr. Sci. 2009, 344, 172–181. [CrossRef] Erdogan, T.; Unveren, E.E.; Inan, T.Y.; Birkan, B. Well-defined block copolymer ionomers and their blend membranes for Lee, W.; Kim, H.; Lee, H. Proton exchange membrane using partially sulfonated polystyrene-b-poly(dimethylsiloxane) for direct exchange membrane fuel cell. J. Membr. Sci. 2009, 344, 172–181. methanol fuel cell. J. Membr. Sci. 2008, 320, 78–85. [CrossRef] Lee, W.; Kim, H.; Lee, H. Proton exchange membrane using partially sulfonated polystyrene-b-poly(dimethylsiloxane) for Ding, J.; Chuy, C.; Holdcroft, S. Enhanced Conductivity in Morphologically Controlled Proton Exchange Membranes: Synthesis methanol fuel cell. J. Membr. Sci. 2008, 320, 78–85. of Macromonomers by SFRP and Their Incorporation into Graft Polymers. Macromolecules 2002, 35, 1348–1355. [CrossRef] 3. 4.DinEgla,bJd.;,CY.hAu.;yW,Calk.;eHr,oCl.dWc.r;oBfety,eSr,.FE.Ln.hTarnibcleodckCcopnodlyumcteirviotynoimneMrmorepmhborlaongeisc:aPlalyrtCII.oSnttrruocltulerdecPhraortaoctnerEizxacthioannagnedMitseemffbecrtasnes:Syn of Monatcraronsmporntopmroepresrtbieys aSnFdRdPiraenctdmTehtheainroIlnfcuoerlpceolrlapteirofnorimnatoncGe.rJa.fMtePmoblry.mScei.r2s0.0M4,a2c3r1o,m18o1le–c1u8l8e.s[C20ro0s2s,R3e5f], 1348–1355. 5. Lee, D.K.; Kim, Y.W.; Choi, J.K.; Min, B.R.; Kim, J.H. Preparation and characterization of proton-conducting crosslinked diblock copolymer membranes. J. Appl. Polym. Sci. 2008, 107, 819–824. [CrossRef] 6. Tsang, E.M.W.; Zhang, Z.; Shi, Z.; Soboleva, T.; Holdcroft, S. Considerations of Macromolecular Structure in the Design of Proton Conducting Polymer Membranes: Graft versus Diblock Polyelectrolytes. J. Am. Chem. Soc. 2007, 129, 15106–15107. [CrossRef] 7. Fisher, A.M. Polymer Electrolyte Membrane and Method of Fabrication. U.S. Patent Application NO. 6,503,378 B1, 7 January 2003. 8. Hofmann, M.A.; Ambler, C.M.; Maher, A.E.; Chalkova, E.; Zhou, X.Y.; Lvov, S.N.; Allcock, H.R. Synthesis of Polyphosphazenes with Sulfonimide Side Groups. Macromolecules 2002, 35, 6490–6493. [CrossRef] 9. Rhim, J.-W.; Park, H.B.; Lee, C.-S.; Jun, J.-H.; Kim, D.S.; Lee, Y.M. Crosslinked poly(vinyl alcohol) membranes containing sulfonic acid group: Proton and methanol transport through membranes. J. Membr. Sci. 2004, 238, 143–151. [CrossRef] 10. Chiang, W.-Y.; Lin, Y.-H. Properties of modified polyacrylonitrile membranes prepared by copolymerization with hydrophilic monomers for water-ethanol mixture separation. J. Appl. Polym. Sci. 2003, 90, 244–250. [CrossRef] 11. Fu, R.Q.; Hong, L.; Lee, J.Y. Membrane Design for Direct Ethanol Fuel Cells: A Hybrid Proton-Conducting Interpenetrating Polymer Network. Fuel Cell 2008, 8, 52–61. [CrossRef] 12. Keller, R.N.; Wycoff, H.D. Copper(I) Chloride. In Inorganic Syntheses; Fernelius, W.C., Ed.; McGraw-Hill Book Company, Inc.: New York, NY, USA, 1946; Volume II. 13. Matyjaszewski, K.; Jo, S.M.; Paik, H.J.; Gaynor, S.G. Synthesis of well-defined polyacrylonitrile by atom transfer radical polymerization. Macromolecules 1997, 30, 6398–6400. [CrossRef] 14. Yang, Y.; Holdcroft, S. Synthetic Strategies for Controlling the Morphology of Proton Conducting Polymer Membranes. Fuel Cell 2005, 5, 171–186. [CrossRef] 15. Mauritz, K.A.; Moore, R.B. State of Understanding of Nafion. Chem. Rev. 2004, 104, 4535–4586. [CrossRef] pPDF Image | Hydrophilic Cross-Linked Aliphatic Hydrocarbon Diblock Copolymer
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