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Method and characterisation Figure 3.22 Modified binding layer with/without inorganic filler in standard electrode assembly The following steps were carried out to prepare the standard binding layer: 0.972 g of Nafion 117 solution (5% in a mixture of lower aliphatic alcohols and water, Sigma-Aldrich ) solution was placed in a vial. 10 ml of acetone was added into the vial and sonicated for 30 minutes. 5.0 ml of the solution was sprayed on the anode electrode using the airbrush at room temperature in the fume hood. The anode electrode was dried in the oven at 100°C for 15 minutes. The same procedures of spraying the binding layer on the anode were followed for the cathode electrode. 3.4.5 Nafion 117 Membrane Activation Nafion 117 membrane sheet (thickness 0.007 in, sigma Aldrich) was only used in this research. The membrane was treated with 1.0 M hydrogen peroxide (H2O2) and 1.0 M of sulfuric acid to oxidize any organic impurities within the membrane and facilitating the proton transportation through the membrane. During the activation, the Sirhan AL-Batty Page 100PDF Image | Membrane Electrode Assembly Modification by Zeolite and Graphene Oxide
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