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Further changes in catalytic performance may also be observed from the conversion versus selectivity plots in Figure 4, determined at maximum levels of conversion. Although both catalysts are almost exclusively selective to the main product, glycidol, up to a peroxide conversion level of 80%, it is clear that TS-1B is able to maintain excellent glycidol selectivity even at substantially higher levels of peroxide conversion. Indeed, whilst glycidol selectivity decreases rapidly to ±85% at 95% conversion with TS-1, glycidol selectivity remains well above 90% throughout the conversion range for TS-1B. This increase in selectivity is certainly non-trivial, atalysts 2015, 5 231 and would allow the conversion to be held at higher levels. Not only does this avoid the formation of unwanted by-products, and hence decreases separation issues, but sues, but it alistoallseoaldesadtoshtoighiegrhseprascpea-cteim-tiem-ye-iyeliedlsdasnadndthteheavaoviodiadnacneceooffuunnneecceesssaarryyrrecycles,, which cou which could improve the potential performance of the system on the whole. This prove the potential performance of the system on the whole. This improved selectivity may be relate improved selectivity may be related to a change in the acid/base character of the a change in the acid/base character of the active sites, to a change in the way H2O2 is activated, or active sites, to a change in the way H2O2 is activated, or to the better availability of e better availability of H2O2 at very high levels of conversion (See below), limiting the ability of t H2O2 at very high levels of conversion (See below), limiting the ability of the active tive sites toscitaetsatloysceattahlyesceotnheseccountsievceutrievaecrteioacnt.ion. Figure 3. Arrhenius plots obtained for (blue squares) TS-1 and (hollow red Figure 3. Arrhenius plots obtained for (blue squares) TS-1 and (hollow red squares) TS-1B. squares) TS-1B. 104 C sl m ot hh cPDF Image | Zeolite Catalysis
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