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Catalysts 2015, 5 2138 capillary condensation step appears at moderate P/P0 (0.2–0.6). A distinct hysteresis loop of H2 type is also clearly observed for both the composites. These phenomena reveal the bimodal-pore properties of comparison with CS-TS-1@mSiO2-30, a higher uptake in the moderate P/P0 of 0.2–0.6 the CS-TS-1@mSiO2 composites from micropores to mesopores as well as the accessible microporous and a more obvious H2 type hysteresis loop in the P/P0 of 0.4–0.6 are apparent for ZSM-5 cores covered with a mesoporous silica shell. Moreover, in comparison with CS-TS-1@mSiO2-30, the CS-TS-1@mSiO2-50, further suggesting the intrinsic bimodal-pore properties a higher uptake in the moderate P/P0 of 0.2–0.6 and a more obvious H2 type hysteresis loop in the P/P0 and the tunable mesopore shells. The pore size distribution (PSD) of pristine of 0.4–0.6 are apparent for the CS-TS-1@mSiO2-50, further suggesting the intrinsic bimodal-pore TS-1 reflects undetectable mesopores and a distinct micropore with a diameter of proper0ti.e5s5anmd.theBtyuncaobnletrmasets,obpotrhesthellsC.ST-hTeS-p1o@remsiSzieOdisthriobwutiotnw(oPSdDis)tionfcptrPisStiDnemTSo-d1elrseflects 2 undeteccotarrbelespmoensdoipnogretsoamndicarodpisotrinecstwmiitchroapsoirme iwlaitrhsiazeditaompetreirstoinf e0.T5S5-1nm(a.rBouyncdon0t.r5a5st,nmbo)th the CS-TSa-n1d@mSeisOop2oshreoswwtwitohdaisBtianrcrtePttS-JDoymnoedr-eHlsacloernrdesapo(BndJHin)gdtoiamiectreorpocreenstewrietdhats2im.6ilnarms,izeto pristinresTpSe-c1ti(vaerolyun(dFi0g.u5r5en3mD))a,nwdhmicehsoinpdoriceastwesitthhaeBfoarmreattt-iJonynoefru-Hnaifloenrmdah(BieJrHar)cdhiiacmaletpeorrceesn.tered BoththeCS-TS-1@mSiO compositesexhibitahighBrunauer-Emmett-Teller(BET) at 2.6 nm, respectively (Figure 3D2 ), which indicates the formation of uniform hierarchical pores. Both surface area of ≥ 550 m2 g−1 of which the microporous surface area was ≥50 m2 g−1 the CS-TS-1@mSiO2 composites exhibit a high Brunauer-Emmett-Teller (BET) surface area of (Ta2ble−11), and a high total pore volume of ≥0.45 m3 g−1.2 Th−1e lower micropore surface ≥ 550 m g of which the microporous surface area was ≥50 m g (Table 1), and a high total pore area was po3ss−i1bly due to presence of a low portion of TS-1 in the composites. All volume of ≥0.45 m g . The lower micropore surface area was possibly due to presence of a low portion the above results indicate that a highly uniform core-shell structured TS-1@mSiO of TS-1 in the composites. All the above results indicate that a highly uniform core-shell structured composite with tunable shell thickness was successfully synthesized via a simple TS-1@mSiO2 composite with tunable shell thickness was successfully synthesized via a simple coating process. coating process. 2 Figure 3. (A) Small-angle XRD patterns of (a) pristine TS-1, (b) CS-TS-1@mSiO -30 Figure 3. (A) Small-angle XRD patterns of (a) pristine TS-1, (b) CS-TS-1@mSiO22-30 and and (c) CS-TS-1@mSiO -50; (B) wide-angle XRD patterns of (a) pristine TS-1, 2 (c) CS-TS-1@mSiO2-50; (B) wide-angle XRD patterns of (a) pristine TS-1, (b) CS-TS-1@mSiO -30 and (c) CS-TS-1@mSiO -50; (C) N sorption isotherms; 222 (b) CS-TS-1@mSiO2-30 and (c) CS-TS-1@mSiO2-50; (C) N2 sorption isotherms; (D) HK and BJH pore size distribution curves. (D) HK and BJH pore size distribution curves. 144PDF Image | Zeolite Catalysis
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