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Author Contributions: Houbing Zou designed the experiments, analyzed the experimental data and wrote the manuscript. Qingli Sun prepared and characterized the samples. Lijia Liu tested the catalytic performances of samples. Weiwei Fu supported the experiments. Dongyu Fan and Runwei Wang revised the final version of paper. Conflicts of Interest: The authors declare no conflict of interest. References 1. Thangaraj, A.; Kumar, R.; Ratnasamy, P. Catalytic Properties of Crystalline Titanium Silicalites II. Hydroxylation of Phenol with Hydrogen Peroxide over TS-1 Zeolites. J. Catal. 1991, 131, 294–297. 2. Martens, J.A.; Buskens, P.; Jacobs, P.A.; van der Pol, A.; van Hooff, J.H.C.; Ferrini, C.; Kouwenhoven, H.W.; Kooyman, P.J.; van Bekkum, H. Hydroxylation of Phenol with Hydrogen Peroxide on EUROTS-1 Catalyst. Appl. Catal. A 1993, 99, 71–84. 3. Hamilton, G.; Friedman, J.; Campbell, P. The Hydroxylation of Anisole by Hydrogen Peroxide in the Presence of Catalytic Amounts of Ferric Ion and Catechol. Scope, Requirements, and Kinetic Studies. J. Am. Chem. Soc. 1966, 88, 5266–5268. 4. Villa, A.; Caro, C.; Correa, C. Cu- and Fe-ZSM-5 as Catalysts for Phenol Hydroxylation. J. Mol. Catal. A 2005, 228, 233–240. 5. Li, B.; Xu, J.; Liu, J.; Zuo, S.; Pan, Z.; Wu, Z. Preparation of Mesoporous Ferrisilicate with High Content of Framework Iron by pH-Modification Method and Its Catalytic Performance. J. Colloid Interface Sci. 2012, 366, 114–119. 6. Choi, J.-S.; Yoon, S.-S.; Jang, S.-H.; Ahn, W.-S. Phenol Hydroxylation Using Fe-MCM-41 Catalysts. Catal. Today 2006, 111, 280–287. 7. Liu, H.; Lu, G.; Guo, Y.; Guo, Y.; Wang, J. Study on the Synthesis and the Catalytic Properties of Fe-HMS Materials in the Hydroxylation of Phenol. Microporous Mesoporous Mater. 2008, 108, 56–64. 8. Fu, W.; Wang, R.; Wu, L.; Wang, H.; Wang, X.; Wang, A.; Zhang, Z.; Qiu, S. Synthesis of Cu2(OH)PO4 Crystals with Various Morphologies and Their Catalytic Activity in Hydroxylation of Phenol. Chem. Lett. 2013, 42, 772–774. 9. Clerici, M.G. Oxidation of Saturated Hydrocarbons with Hydrogen Peroxide Catalysed by Titanium Silicalite. Appl. Catal. 1991, 68, 249–261. 10. Xiao, F.; Han, Y.; Yu, Y.; Meng, X.; Yang, M.; Wu, S. Hydrothermally Stable Ordered Mesoporous Titanosilicates with Highly Active Catalytic Sites. J. Am. Chem. Soc. 2002, 133, 888–889. 11. Lin, K.; Wang, L.; Meng, F.; Sun, Z.; Yang, Q.; Cui, Y.; Jiang, D.; Xiao, F.S. Formation of Better Catalytically Active Titanium Species in Ti-MCM-41 by Vapor-phase Silylation. J. Catal. 2005, 235, 423–427. 12. Tsai, S.-T.; Chao, P.-Y.; Tsai, T.-C.; Wang, I.; Liu, X.; Guo, X.-W. Effects of Pore Structure of Post-treated TS-1 on Phenol Hydroxylation. Catal. Today 2009, 148, 174–178. 13. Zhu, G.; Ni, L.; Qi, W.; Ding, S.; Li, X.; Wang, R. Synthesis and Morphology Research of Framework Ti-rich TS-1 Containing No Extraframework Ti Species in the Presence of CO2. Inorg. Chem. Commun. 2014, 40, 129–132. 151PDF Image | Zeolite Catalysis
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