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Catalysts 2016, 6, 13 4 of 12 The EDAX elemental maps present the element distribution of Si, O, Al, and Ga (Figure 4), and bright greCeantadlyosttss2i0n16d,i6c,a13testhatGaelementiswelldispersedontheas-preparedGa2O3/ZSM-5hollow4foifb1e2rs. The EDAX elemental maps present the element distribution of Si, O, Al, and Ga (Figure 4), and bright green dots indicates that Ga element is well dispersed on the as-prepared Ga2O3/ZSM-5 hollow fibers. (A) (B) (C) (A) (B) (C) (D) (E) (F) Figure 3. SEM images of the as-prepared Nano-ZSM-5 (A); 0.3% Ga2O3/ZSM-5 (B); 0.3% Ga2O3/ZSM- (D) (E) (F) Figure 3. SEM images of the as-prepared Nano-ZSM-5 (A); 0.3% Ga O /ZSM-5 (B); 23 5/PVP fibers before calcination (C); the low (D) and magnified (E) SEM images of 0.3% Ga2O3/ZSM-5 Figure 3. SEM images of the as-prepared Nano-ZSM-5 (A); 0.3% Ga2O3/ZSM-5 (B); 0.3% Ga2O3/ZSM- 0.3% Ga O /ZSM-5/PVP fibers before calcination (C); the low (D) and magnified hollow fibers after calcination at 550 °C, respectively; TEM image (F) of one hollow fiber after 23 5/PVP fibers before calcination (C); the low (D) and magnified (E) SEM images of 0.3% Ga2O3/Z ̋SM-5 (E) SEM images of 0.3% Ga O /ZSM-5 hollow fibers after calcination at 550 C, calcination at 550 °C. hollow fibers after calcination at 550 °C, respectively; TEM image (F) of one hollow fiber after 23 respectively; TEM image (F) of one hollow fiber after calcination at 550 ̋C. calcination at 550 °C. Figure 4. EDAX elemental maps of Si, O, Al, and Ga of 0.3% Ga2O3/ZSM-5 zeolite hollow fibers. Figure 4. EDAX elemental maps of Si, O, Al, and Ga of 0.3% Ga2O3/ZSM-5 zeolite hollow fibers. Figure 4. EDAX elemental maps of Si, O, Al, and Ga of 0.3% Ga2O3/ZSM-5 zeolite Figure 5 shows the nitrogen adsorption-desorption isotherms and BJH pore size distribution Figure 5 shows the nitrogen adsorption-desorption isotherms and BJH pore size distribution hollow fibers. (inset) of the Ga2O3/ZSM-5 hollow fibers. According to the nitrogen adsorption-desorption (inset) of the Ga2O3/ZSM-5 hollow fibers. According to the nitrogen adsorption-desorption measurement, the Brunauer-Emmett-Teller (BET) surface area of 377 m2 2/g and the pore volume of measurement, the Brunauer-Emmett-Teller (BET) surface area of 377 m /g and the pore volume of Figure 5 shows the nitrogen adsorption-desorption isotherms and BJH pore size 0.275 cm3/g3were determined. From Figure 5, it can be seen that the present isotherms exhibit a typical 0.275 cm /g were determined. From Figure 5, it can be seen that the present isotherms exhibit a typical distribution (inset) of the Ga O /ZSM-5 hollow fibers. According to the nitrogen 23 hysteresis loop at p/p0 > 0.1, indicating mesopores are formed, arising from the interparticle voids of hysteresis loop at p/p0 > 0.1, indicating mesopores are formed, arising from the interparticle voids of Ga2GOa32/OZ3S/MZS-M5.-5H. eHnecnec, et,hteheasa-sp-rperpeparaerded GGaa2O2O33//ZSM-5 hollow ffiibeerrss eexxhhibibititaagogododhiheriearcahrcichailcal macmroac-mroe-msoe-smo-imcriocproprorsoitsyit,y,wwithithmmicircoroppoorreessiinZSM-5 nanoparrttiiccleless,,meesosopporoersesfofromrmededbybythethe stacsktainckginogf tohfethGeaG2Oa23O/Z3/SZMSM-5-5nannaonpoparatritcilceless,,aannd1co8on1ntinuous macropoorreessoonnththeehohlolollwowfibfiebres.rs.PDF Image | Zeolite Catalysis
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