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ADVANCED MICROTURBINE SYSTEMS Final Report for Tasks 1 Through 4 and Task 6

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ADVANCED MICROTURBINE SYSTEMS Final Report for Tasks 1 Through 4 and Task 6 ( advanced-microturbine-systems-final-report-tasks-1-through-4 )

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99.00 90.00 50.00 10.00 5.00 As received Si3N4, m=12.5, σc=86.7 ksi, R2=0.97 Si3N4 with new bond coat system, m=10.3, σc=86.9 ksi, R2=0.93 1.00 50.00 100.0 Bend Strength, Figure 4.2.6: Strength of samples fractured in four point bending shown as Weibull distribution The Weibull modulus and characteristic strength for the as received silicon nitride samples are 12.5 and 86.7 ksi, respectively. The Weibull modulus and characteristic strength for silicon nitride with bond coat system are 10.3 and 86.9 ksi, respectively. The distributions of the two sets of data are similar both in magnitude and in scatter. The regression analysis shows similar degree of fit for both sets of samples as judged from the R2 value. The Weibull analysis suggests that both sets of samples contain strength- controlling flaws of nearly the same size and distribution. Fractographic analysis indicates that the nature of strength-limiting flaws in the uncoated substrate and the substrate with the bond coat system remains unchanged. Figures 4.2.7(a) and (b) show fracture surfaces of coated and uncoated SN282 as observed under a low magnification stereo microscope. The failure strength of as received silicon nitride is 86.6 ksi, while the failure strength of the coated silicon nitride is 81.4 ksi. The fracture origin for both samples, as marked in the Figure 4.2.7, is from the silicon nitride surface as judged by the fracture mirror and crack branching pattern. The magnitude of fracture mirror radius is also approximately the same for both the samples (~ 300μm). 88 Prob. of Failure

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