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Subtask 3-3-2 Composition of Corrosion Products a) b) Figure 4-18. The corrosion product at spot 1 (blue circle in a)) that forms on I-617 in supercritical CO2 at 1000oC is composed mainly of chromium oxide as shown by the EDS spectra in b). (The unidentified peaks are from a conductive gold coating applied after exposure.) EDS chemical analysis was used to get a qualitative composition of the corrosion products in Figure 4-17a. Chemical analysis of the corroded intergranular areas was performed on the SEM. Figures 4-18a & 4-18b shows the areas of analysis and the EDS spectra obtained from spot 1, respectively. It is evident from Fig. 4-18b that the corrosion product is composed exclusively of chromium oxide. (The rather large unidentified peaks correspond to gold which was used to coat the sample to make the corrosion products more conductive and enable SEM to be performed.) Again, chromium oxide is the only thermodynamically stable corrosion product at 1000oC. (It should be pointed out that many forms of 74PDF Image | Development Of A Supercritical Carbon Dioxide Brayton Cycle
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