RECOVERY OF BUTANOL

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RECOVERY OF BUTANOL ( recovery-butanol )

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WATER N4C6 CO2 Mass Frac 36252.825 1176.597 36252.805 28000 1176.604 1189.746 35063.078 36252.825 23641.697 23103.345 21885.117 5496.512 27381.629 trace 354.038 822.559 1176.597 656.714 trace 29 27381.63 28000 30 ETOH 0.162 I-BUOH 0.374 OLEYLOH WATER N4C6 1 1 CO2 0.015 0.12 0.054 0.142 0.121 0.01 22 PPB 0.054 100 PPM 0.863 0.925 0.072 0.075 trace 0.002 trace Temperature C. Pressure atm Vapor Frac Mole FloW kmol/hr Mass FloW kg/hr Volume FloW l/hr Enthalpy MMBtu/hr Mass FloW kg/hr ETOH I-BUOH OLEYLOH WATER N4C6 trace CO2 trace 656.714 Mass Frac ETOH 22PPB I-BUOH 100PPM OLEYLOH 0.925 WATER 0.075 N4C6 trace 0.01 0.054 0.863 0.072 618.35 27356.423 656.721 442.547 0.021 0.098 0.015 0.401 trace 312 PPM 0.017 0.036 0.459 0.458 0.488 0.007 25.227 77.336 0.15 0.131 947 PPB 5471.285 21885.138 88.509 354.038 0.098 0.098 0.401 0.401 312 PPM 312 PPM 0.021 trace 0.152 0.824 695 PPM CO2 Temper- ature trace 0.002 TABLE13 0.717 0.036 0.036 0.024 530 PPM 0.458 0.458 1000 PPB 0.002 0.007 0.007 trace 0.007 3284.882 30.779 17731.273 1170.868 4683.47 3256.362 4789.326 19157.304 17680.269 284670.51 284685.43 23103.345 23641.697 28.134 5854.338 7145.064 20.141 23946.63 6207.912 trace 18.652 0.045 3.73 14.922 14.922 SimulatedBUOH ColumnTrafficandLiquidMass CompositionPro?leOutputsforExample4. Heat Liquid Vapor Liquid Vapor Pressure duty floW floW feed feed Stage C. atm MJ/hr kg/hr kghr kg/hr kg/hr 1 58.8677 2 59.54895 3 59.65739 4 59.75322 5 59.84637 6 59.93224 7 59.99611 8 60.02964 9 61.89011 10 78.22766 11 86.2438 12 87.59943 13 88.42887 14 90.35375 15 94.95595 0.986923 0 0.990448 0 0.993973 0 0.997497 0 1.001022 0 1.004547 0 1.008072 0 1.011596 0 1.015121 0 1.018646 0 1.022171 0 1.025695 0 1.02922 0 1.032745 0 1.036269 17905.467 53619.022 53793.603 53804.133 53811.405 53818.989 53827.699 53834.924 53227.389 43249.936 39494.953 39676.2 40017.329 40932.433 43270.946 21466.802 26333.043 47724.677 32152.221 0 0 32326.802 0 0 32337.332 0 0 32344.603 0 0 32352.188 0 0 32360.898 0 0 32368.122 0 0 31760.587 0 0 21783.134 0 0 18028.151 0 0 18209.398 0 0 18550.528 0 0 19465.631 0 0 21804.144 0 0 Mixed Liquid Vapor feed product product 1stliquid 2ndliquid Stage kghr kghr kg/hr floWkg/hr floWkghr 1 0 2 0 3 0 4 0 5 0 6 0 7 0 8 0 0 26333.043 0 0 0 0 0 0 0 0 0 0 0 0 0 0 41870.422 41980.297 41974.264 41964.857 41952.005 41928.534 41880.218 41103.791 11748.6 11813.306 11829.869 11846.548 11866.984 11899.165 11954.706 12123.598 US 8,563,788B2 TABLE 12-c0ntinued Simulated Stream Outputs for Example 4. 0.278 0.056 0.351 0.279 232PPM 172PPM 1PPB 229PPM 173PPM 42 85.4 1.09 1.05 0 0.003 2343.146 2698.119 307804.64 330000 3658639 602048.47 —881.463 —956.96 35 1 24.263 1346.45 35 35 35 35 95 1 1 1 1 1.04 0 0 0 0 <0.001 896.043 2133.581 179.209 716.835 337.876 59749.806 47554.068 11949.961 47799.845 21466.802 83180.38 51387.885 16636.076 66544.304 29143.379 0.45 0.334 0.045 0.429 0.258 0.831 0.067 0.011 0.013 0.01 0.336 0.253 0.011 42 43 46 47 48 49 50 60 —229.936 —578.686 —45.987 —183.949 —97.749 23.105 2131.216 34098.483 426.243 1704.973 515.227 75.167578

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